Imidazole added sulphamic acid single crystals with optimal properties for optoelectric devices

Author(s):  
S. Anciya ◽  
A.S.I. Joy Sinthiya ◽  
P. Selvarajan ◽  
R. Sree Devi
2018 ◽  
Vol 15 (2) ◽  
pp. 151-158 ◽  
Author(s):  
K.G. Anupriya ◽  
P. Hemalatha

Single crystals of Sulphamic Acid doped with Zinc Sulphate and Manganese Sulphate were grown at room temperature using slow evaporation technique. Structural analysis of the grown crystals was done using single crystal X Ray Diffraction and powder X Ray Diffraction studies. Various functional groups seen in the grown crystals are determined using FTIR spectroscopic analysis. The cut-off wavelength of ZnSO4 and MnSO4 doped Sulphamic acid were evaluated by UV-Vis-NIR spectral studies. Thermal behaviour of the grown crystals was identified from Thermogravimetric Analysis (TGA) and Differential Thermogravimetric Analysis (DTA). The mechanical strength and Second harmonic generation of the grown crystals was identified by Vicker’s Microhardness Test and Kurtz powder technique respectively.


2016 ◽  
Author(s):  
S. Rajyalakshmi ◽  
Valluru Srinivasa Rao ◽  
P. V. S. S. S. N. Reddy ◽  
V. Y. Rama Krishna ◽  
K. Samatha ◽  
...  

2014 ◽  
Vol 2014 ◽  
pp. 1-5 ◽  
Author(s):  
D. Jaishree ◽  
G. Kanchana ◽  
R. Kesavasamy

Single crystals of sulphamic acid of 11 × 7 × 3 mm3dimension were successfully grown by slow evaporation technique. The crystal structure of grown crystals was confirmed by single crystal X-ray diffraction analysis. The presence of functional groups in the crystal lattice has been qualitatively determined by FT-IR and FT-Raman analyses. Theoretical group factor analysis predicts the possible modes of vibrations. The optical transmission spectroscopy (UV-Vis) clearly evidences the suitability of this material for optical application. The thermal behaviour of the crystal was studied by thermogravimetric (TG) and differential scanning calorimetric (DSC) studies. The nonlinear optical (NLO) characteristic of this material was explored by the second harmonic generation (SHG) conversion efficiency.


Heliyon ◽  
2019 ◽  
Vol 5 (7) ◽  
pp. e01988 ◽  
Author(s):  
J. Arumugam ◽  
N. Suresh ◽  
M. Selvapandiyan ◽  
S. Sudhakar ◽  
M. Prasath

2015 ◽  
Vol 27 (7) ◽  
pp. 2642-2646
Author(s):  
R. Sreedevi ◽  
K. Amarsingh Babu ◽  
T. Balu ◽  
P. Murugakoothan ◽  
T.R. Rajasekaran

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