Direct analysis of annealing of nodular crystals in isotactic polypropylene by atomic force microscopy, and its correlation with calorimetric data

Polymer ◽  
2007 ◽  
Vol 48 (12) ◽  
pp. 3504-3511 ◽  
Author(s):  
Qamer Zia ◽  
Hans-Joachim Radusch ◽  
René Androsch
Polymer ◽  
2021 ◽  
pp. 124445
Author(s):  
Jiugeng Cheng ◽  
Zhenxing Zhong ◽  
Yuan Lin ◽  
Zhaohui Su ◽  
Chunyu Zhang ◽  
...  

2006 ◽  
Vol 285 (4) ◽  
pp. 449-455 ◽  
Author(s):  
Xi Wang ◽  
Weimin Hou ◽  
Jianjun Zhou ◽  
Lin Li ◽  
Yang Li ◽  
...  

1993 ◽  
Vol 26 (22) ◽  
pp. 5915-5923 ◽  
Author(s):  
W. Stocker ◽  
S. N. Magonov ◽  
H. J. Cantow ◽  
J. C. Wittmann ◽  
B. Lotz

1998 ◽  
Vol 13 (1) ◽  
pp. 223-227 ◽  
Author(s):  
A. Dias ◽  
R. L. Moreira ◽  
N. D. S. Mohallem ◽  
J. M. C. Vilela ◽  
M. S. Andrade

Atomic force microscopy, as well as the Brunauer, Emmett, and Teller technique and x-ray diffraction, was used to analyze ultrafine NiZn ferrite powders hydrothermally synthesized at 200 °C, for 5 h. The particle sizes, measured through AFM images acquired from the surface of pressed powders, were 52 ± 6 nm, which were higher than those obtained by the other techniques. The particles were monodispersed in size and approximately spherical, meeting the requirements for the production of high density sintered components. The observations performed on ceramic bodies sintered at different conditions (1100–1400 °C, 5 to 240 min) showed necks characteristic of the early stages of sintering (1100 °C) and the expected pore curvature evolution (1400 °C) with sintering time in the final stage of the sintering process. Using a straightforward sample preparation technique, AFM proved to be a powerful tool for direct analysis of ceramic powder particles on the nanometric scale and sintered ceramics at different sintering stages.


Polymer ◽  
2016 ◽  
Vol 82 ◽  
pp. 349-355 ◽  
Author(s):  
Kiminori Uchida ◽  
Kazuki Mita ◽  
Osamu Matsuoka ◽  
Takeharu Isaki ◽  
Kenjiro Kimura ◽  
...  

Polymer ◽  
2005 ◽  
Vol 46 (12) ◽  
pp. 4077-4087 ◽  
Author(s):  
Jian-Jun Zhou ◽  
Ji-Guang Liu ◽  
Shou-Ke Yan ◽  
Jin-Yong Dong ◽  
Lin Li ◽  
...  

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