Ultrasound-assisted synthesis of substituted guanidines using 1 H -pyrazole-1-carboxamidine and S -methylisothiouronium sulfate under solvent-free conditions

Tetrahedron ◽  
2018 ◽  
Vol 74 (32) ◽  
pp. 4339-4342 ◽  
Author(s):  
Mitsue Fujita ◽  
Yoshio Furusho
2016 ◽  
Vol 42 (6) ◽  
pp. 5993-6002 ◽  
Author(s):  
Abdeslem Bouzina ◽  
Nour-eddine Aouf ◽  
Malika Berredjem

2012 ◽  
Vol 77 (4) ◽  
pp. 415-421 ◽  
Author(s):  
Masoud Nasr-Esfahani ◽  
Morteza Montazerozohori ◽  
Najmeh Filvan

A rapid and convenient preparation of acyclic imides by the reaction of aliphatic and aromatic nitriles with acyclic carboxylic anhydride in the presence of catalytic amounts of p-toluenesulfonic acid under thermal or ultrasonic conditions is reported. The advantages of this procedure are moderate reaction times, good to excellent yields, use of inexpensive and ecofriendly catalyst. The reaction of nitriles with aliphatic anhydrides proceeds in thermal conditions, while by the use of ultrasound irradiations these reactions get accelerated.


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