A reversed-phase high performance liquid chromatography method using solid phase extraction to quantitate thalidomide in human serum

1997 ◽  
Vol 339 (1-2) ◽  
pp. 91-97 ◽  
Author(s):  
Bradley R. Simmons ◽  
Richard M. Lush ◽  
William D. Figg
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Solid Phase Extraction ◽  
Human Serum ◽  
High Performance ◽  
Solid Phase ◽  
Reversed Phase ◽  
Phase Extraction ◽  
Chromatography Method ◽  
Liquid Chromatography Method

Aquatic Products Determination of Nonylphenol and Octylphenol

2013 ◽  
Vol 340 ◽  
pp. 388-391 ◽  
Author(s):  
Xiang Ke Cao ◽  
Qing Zeng Qian ◽  
Jun Wang Tong ◽  
Qian Wang
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Solid Phase Extraction ◽  
High Performance ◽  
Solid Phase ◽  
Phase Extraction ◽  
Chromatography Method ◽  
Aquatic Product ◽  
Liquid Chromatography Method

By solid - phase extraction high performance liquid chromatography determination of nonylphenol, Octylphenol in aquatic product residues, to establish more accurate, fast, effective detection method. Sample is 3 trichloroacetic acid solution after extraction, using anion exchange solid phase extraction column purification by reversed phase high performance liquid chromatography method for determination. Column is Shim-pack VP-ODS 250mm x4.6mm, detection wavelength is225 nm, mobile phase of methanol - water ( volume ratio of 75:25), flow rate is 0.8 mL/min, injection volume is 20 ìL. Octylphenol, nonylphenol respectively in 0.14¡«97.63 ìg/mL ( R=0.9995),0.02¡«51.04 ì g/mL ( R=0.9997) concentration and peak area show a good linear relationship, octylphenol nonylphenol and the recovery is 87.9%¡«93.8%, relative standard deviation is 1.4%¡«3.8%. Solid - phase extraction high performance liquid chromatography method for determination of aquatic product of octylphenol and nonylphenol residue is accurate, rapid, high sensitivity, suitable for aquatic products of octylphenol nonylphenol and detection.

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