Ion-exchange separation and quantitative determination of dimethyl sulfoxide

1967 ◽  
Vol 26 ◽  
pp. 336-338 ◽  
Author(s):  
L.H. Krull ◽  
Mendel Friedman
1957 ◽  
Vol 3 (3) ◽  
pp. 169-177 ◽  
Author(s):  
Bernard Shapiro ◽  
David Seligson ◽  
Ralph Jessar

Abstract A new method for the measurement of uric acid in biologic fluids is presented. It involves the isolation of uric acid by ion-exchange separation and quantitative determination of uric acid in the eluate by ultraviolet absorption, the Folin-Brown method or an enzymatic technic. The enzymatic determination on the eluate is the most specific of the technics. A series of determinations of uric acid in serum compares well with determinations on the same samples using the direct Folin-Brown procedure. The direct Folin-Brown method appears to be in error in determinations on certain urine samples. Measurements of uric acid in bile are reported. The technic can be used in the routine clinical laboratory, and is particularly applicable to fluids which cannot be studied by direct methods.


2004 ◽  
Vol 90 (1) ◽  
pp. 48-50 ◽  
Author(s):  
Hitoshi YAMAGUCHI ◽  
Shinji ITOH ◽  
Shin'ichi HASEGAWA ◽  
Kunikazu IDE ◽  
Takeshi KOBAYASHI

1977 ◽  
Vol 49 (11) ◽  
pp. 1595-1598 ◽  
Author(s):  
Michael D. Arguello ◽  
James S. Fritz

1971 ◽  
Vol 54 (4) ◽  
pp. 790-795
Author(s):  
C E Jones ◽  
L E Pracht

Abstract This collaborative study represents an attempt to validate the ion exchange zincon method for the quantitative determination of zinc in fertilizers. The values of the standard deviations Sd, Sr, and Sb and the results of the F- and t-tests are presented as an estimate of the precision, accuracy, and dependability. Atomic absorption measurements were also made and provided reference data for evaluation purposes. In its present form, the method falls short of expectations as an alternative wet approach to the dithizone method. It is recommended that the methods for determining zinc in fertilizers be studied further.


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