Synthesis and Characterization of New Soluble Polyimides from 3,3‘,4,4‘-Benzhydrol Tetracarboxylic Dianhydride and Various Diamines

1998 ◽  
Vol 10 (3) ◽  
pp. 734-739 ◽  
Author(s):  
Der-Jang Liaw ◽  
Been-Yang Liaw ◽  
Lain-Jong Li ◽  
Bernard Sillion ◽  
Régis Mercier ◽  
...  

2005 ◽  
Vol 96 (6) ◽  
pp. 2300-2308 ◽  
Author(s):  
Sung Mook Choi ◽  
Kyung Jun Kim ◽  
Kil-Yeong Choi ◽  
Mi Hye Yi


RSC Advances ◽  
2018 ◽  
Vol 8 (56) ◽  
pp. 31881-31888
Author(s):  
R. Sulub-Sulub ◽  
M. I. Loría-Bastarrachea ◽  
J. L. Santiago-García ◽  
M. Aguilar-Vega

Three new polyimides were synthesized from 3,8-diphenylpyrene-1,2,6,7-tetracarboxylic dianhydride (DPPD) with two diamines with ortho methyl substitution (MBDAM and HFI) and one diamine without ortho substituents (BAPHF).



2011 ◽  
Vol 415-417 ◽  
pp. 1789-1793
Author(s):  
Xiang Li Meng ◽  
Peng Wang ◽  
Ling Jiang

Polyimides prepared from 5-amino-2(p-aminophenyl) benzoxazole (AAPB) with pyromellitic dianhydride(PMDA), 2,2’3,3’-biphenyl tetracarboxylic dianhydride(i-BPDA), 4,4’-oxdiphthalic anhydride(ODPA), 1,4-bis(3,4-dicarbosyphenoxy) benzene dianhydride(HQDPA) and 2,2-bis(3,4-dicarboxyphenyl)hexafluoropropane dianhydride (6FDA) were synthesized successfully via a conventional two-stage method. Their structures and properties were characterized by FT-IR, DSC, TG and XRD. The intermediate poly(amic acid)s had inherent viscosity range of 0.86~2.18 dL/g and could be thermally converted into light yellow polyimide films. The polyimides showed excellent solvent resistance and good thermal stability. The glass transition temperatures (Tg) were found to be 336oC~369 oC .The decomposition started at a temperature above 530oC in N2 atmosphere.





1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula


2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.



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