Rapid and Simultaneous Determination of Essential Minerals and Trace Elements in Human Milk by Improved Flame Atomic Absorption Spectroscopy (FAAS) with Microwave Digestion

2010 ◽  
Vol 58 (17) ◽  
pp. 9396-9400 ◽  
Author(s):  
Yang Luo ◽  
Bo Zhang ◽  
Ming Chen ◽  
Jue Wang ◽  
Xue Zhang ◽  
...  
1981 ◽  
Vol 35 (5) ◽  
pp. 502-505 ◽  
Author(s):  
J. J. Labrecque ◽  
D. Adames ◽  
W. C. Parker

A rapid method is presented for the simultaneous determinations of thorium, niobium, lead, and zinc in lateritic material from Cerro Impacto, Estado Bolívar, Venezuela. This technique uses a PDP—11/05 processor—based photon induced x-ray fluorescence system. The total variations of approximately 5% for concentrations of approximately 1 and 10% for concentrations of approximately 0.1% were obtained with only 500 s of fluorescent time. The values obtained by this method were in agreement with values measured by conventional flame atomic absorption spectroscopy for lead and zinc. The values for thorium measured were in agreement with the reported values for the reference materials supplied by NBL.


1986 ◽  
Vol 69 (5) ◽  
pp. 871-873
Author(s):  
M Jesus Alvarez de Eulate ◽  
Rosa Montoro ◽  
Nieves Ybañez ◽  
Miguel De La Guardia

Abstract A method for determination of Cd, Cu, and Pb in sodium chloride food salt samples has been developed. It consists of extraction in 4- methj 1-2-pentanonc of the complexes formed with ammonium pyrrolidine dithiocarbamate and further analysis of the extracts by flame atomic absorption spectroscopy. Detection limits in ng/g salt were 0.2 for Cd, 0.7 for Cu, and 10.0 for Pb. The coefficients of variation of 12 independent analyses were 13% for Cd (at a level of 0.4 ppb), 18% for Cu (1.6 ppb), and 5% for Pb (40 ppb). The recoveries were 100 ± 0% for Cd, 115 ± 14% for Cu, and 100 ± 13% for Pb.


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