A Facile One-Pot Synthesis of Alkyl Aryl Sulfides from Aryl Bromides

2004 ◽  
Vol 69 (9) ◽  
pp. 3236-3239 ◽  
Author(s):  
Jungyeob Ham ◽  
Inho Yang ◽  
Heonjoong Kang
Keyword(s):  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis ◽  
Aryl Bromides ◽  
Aryl Sulfides

scholarly journals A Facile One-Pot Synthesis of Alkyl Aryl Sulfides from Aryl Bromides.

ChemInform ◽  
2004 ◽  
Vol 35 (35) ◽  
Author(s):  
Jungyeob Ham ◽  
Inho Yang ◽  
Heonjoong Kang
Keyword(s):  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis ◽  
Aryl Bromides ◽  
Aryl Sulfides

scholarly journals Efficient Cu-catalyzed base-free C–S coupling under conventional and microwave heating. A simple access to S-heterocycles and sulfides

2013 ◽  
Vol 9 ◽  
pp. 467-475 ◽  
Author(s):  
Silvia M Soria-Castro ◽  
Alicia B Peñéñory
Keyword(s):  
Microwave Irradiation ◽  
Microwave Heating ◽  
Catalytic System ◽  
Low Cost ◽  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis ◽  
Aryl Iodides ◽  
The One ◽  
Aryl Sulfides

S-aryl thioacetates can be prepared by reaction of inexpensive potassium thioacetate with both electron-rich and electron-poor aryl iodides under a base-free copper/ligand catalytic system. CuI as copper source affords S-aryl thioacetates in good to excellent yields, by using 1,10-phenanthroline as a ligand in toluene at 100 °C after 24 h. Under microwave irradiation the time was drastically reduced to 2 h. Both procedures are simple and involve a low-cost catalytic system. This methodology was also applied to the “one-pot” synthesis of target heterocycles, such as 3H-benzo[c][1,2]dithiol-3-one and 2-methylbenzothiazole, alkyl aryl sulfides, diaryl disulfides and asymmetric diaryl sulfides in good yields.

Copper-Catalyzed Three-Component Coupling Reaction of Aryl Iodides, a Disilathiane, and Alkyl Benzoates Leading to a One-Pot Synthesis of Alkyl Aryl Sulfides

Synthesis ◽  
2019 ◽  
Vol 51 (11) ◽  
pp. 2323-2330
Author(s):  
Norio Sakai ◽  
Hiromu Maeda ◽  
Yohei Ogiwara
Keyword(s):  
Coupling Reaction ◽  
Sulfur Source ◽  
Diphenyl Diselenide ◽  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis ◽  
Aryl Iodides ◽  
Alkyl Moiety ◽  
Aryl Sulfides ◽  
Three Component Coupling

A copper-catalyzed three-component coupling reaction of aryl iodides, hexamethyldisilathiane and alkyl benzoates leading to alkyl aryl sulfides has been demonstrated. A disilathiane acted as both a sulfur source and a promoter of the sulfidation, and the alkyl moiety of the alkyl benzoate was effectively introduced on one side of the sulfide. Moreover, we found that the protocol can be expanded to the preparation of ethyl phenyl selenide with diphenyl diselenide.

ChemInform Abstract: Nanodomain Cubic Cuprous Oxide as Reusable Catalyst in One-Pot Synthesis of 3-Alkyl/Aryl-3- (pyrrole-2-yl/indole-3-yl)-2-phenyl-2,3-dihydro-isoindolinones in Aqueous Medium.

ChemInform ◽  
2014 ◽  
Vol 45 (41) ◽  
pp. no-no
Author(s):  
Swarbhanu Sarkar ◽  
Nivedita Chatterjee ◽  
Manas Roy ◽  
Rammyani Pal ◽  
Sabyasachi Sarkar ◽  
...  
Keyword(s):  
Aqueous Medium ◽  
Cuprous Oxide ◽  
Reusable Catalyst ◽  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis

One-Pot Synthesis of Symmetrical and Unsymmetrical Aryl Sulfides by Pd-Catalyzed Couplings of Aryl Halides and Thioacetates

2011 ◽  
Vol 76 (11) ◽  
pp. 4371-4378 ◽  
Author(s):  
Namjin Park ◽  
Kyungho Park ◽  
Mihee Jang ◽  
Sunwoo Lee
Keyword(s):  
Aryl Halides ◽  
One Pot ◽  
One Pot Synthesis ◽  
Aryl Sulfides

One-Pot Synthesis of Amine-Substituted Aryl Sulfides and Benzo[b]thiophene Derivatives

2010 ◽  
Vol 12 (10) ◽  
pp. 2430-2433 ◽  
Author(s):  
Zhongyu Duan ◽  
Sadananda Ranjit ◽  
Xiaogang Liu
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
Thiophene Derivatives ◽  
Aryl Sulfides

ChemInform Abstract: HMPA Mediated One-Pot Synthesis of 1-Alkyl/Aryl-4-dimethylamino[1,2,4]triazalo[4,3-a]quinoxalines.

ChemInform ◽  
2001 ◽  
Vol 32 (3) ◽  
pp. no-no
Author(s):  
V. S. H. Krishnan ◽  
K. S. Chowdary ◽  
P. K. Dubey
Keyword(s):  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis

Plasma synthesis of oxidized graphene foam supporting Pd nanoparticles as a new catalyst for one-pot synthesis of dibenzyls

RSC Advances ◽  
2014 ◽  
Vol 4 (108) ◽  
pp. 63048-63054 ◽  
Author(s):  
Liang Ren ◽  
Fan Yang ◽  
Chunxia Wang ◽  
Yongfeng Li ◽  
Hailing Liu ◽  
...  
Keyword(s):  
Pd Nanoparticles ◽  
Plasma Synthesis ◽  
One Pot ◽  
Graphene Foam ◽  
Plasma Method ◽  
One Pot Synthesis ◽  
Aryl Bromides

Pd nanoparticles decorated oxidized graphene foam (Pd/OGF) has been prepared by a gas–liquid interfacial plasma method and successfully used for one-pot synthesis of dibenzyls with different aryl bromides and olefins.

Palladium catalyzed decarboxylative acylation of arylboronic acid with ethyl cyanoacetate as a new acylating agent: synthesis of alkyl aryl ketones

2015 ◽  
Vol 39 (11) ◽  
pp. 8763-8770 ◽  
Author(s):  
Md Yousuf ◽  
Tuluma Das ◽  
Susanta Adhikari
Keyword(s):  
Ethyl Cyanoacetate ◽  
Acylating Agent ◽  
Arylboronic Acid ◽  
One Pot ◽  
Alkyl Aryl ◽  
One Pot Synthesis ◽  
Aryl Ketones ◽  
Palladium Catalyzed

The versatile, one-pot synthesis of a series of alkyl aryl ketones is described using ethyl cyanoacetate as a new acylating agent.

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