Determination of Molecular Geometry in Solid-State NMR:  Rotational-Echo Double Resonance of Three-Spin Systems

2003 ◽  
Vol 107 (5) ◽  
pp. 1272-1283 ◽  
Author(s):  
Frederick G. Vogt ◽  
James M. Gibson ◽  
Sue M. Mattingly ◽  
Karl T. Mueller
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Double Resonance ◽  
Molecular Geometry ◽  
Spin Systems ◽  
Rotational Echo Double Resonance

Determination of Molecular Geometry by High-Order Multiple-Quantum Evolution in Solid-State NMR

2000 ◽  
Vol 144 (2) ◽  
pp. 266-279 ◽  
Author(s):  
Mattias Edén ◽  
Andreas Brinkmann ◽  
Henrik Luthman ◽  
Lars Eriksson ◽  
Malcolm H Levitt
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Molecular Geometry ◽  
High Order ◽  
Quantum Evolution ◽  
Multiple Quantum

scholarly journals Use of Solid-State NMR Spectroscopy for the Characterization of Molecular Structure and Dynamics in Solid Polymer and Hybrid Electrolytes

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1207
Author(s):  
Gabrielle Foran ◽  
Nina Verdier ◽  
David Lepage ◽  
Cédric Malveau ◽  
Nicolas Dupré ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Pulse Sequence ◽  
Dynamic Properties ◽  
Double Resonance ◽  
Solid Polymer ◽  
Pulse Field ◽  
Solid State Nmr Spectroscopy

Solid-state NMR spectroscopy is an established experimental technique which is used for the characterization of structural and dynamic properties of materials in their native state. Many types of solid-state NMR experiments have been used to characterize both lithium-based and sodium-based solid polymer and polymer–ceramic hybrid electrolyte materials. This review describes several solid-state NMR experiments that are commonly employed in the analysis of these systems: pulse field gradient NMR, electrophoretic NMR, variable temperature T1 relaxation, T2 relaxation and linewidth analysis, exchange spectroscopy, cross polarization, Rotational Echo Double Resonance, and isotope enrichment. In this review, each technique is introduced with a short description of the pulse sequence, and examples of experiments that have been performed in real solid-state polymer and/or hybrid electrolyte systems are provided. The results and conclusions of these experiments are discussed to inform readers of the strengths and weaknesses of each technique when applied to polymer and hybrid electrolyte systems. It is anticipated that this review may be used to aid in the selection of solid-state NMR experiments for the analysis of these systems.

scholarly journals Structure determination of molecular nanocomposites by combining pair distribution function analysis and solid-state NMR

RSC Advances ◽  
2015 ◽  
Vol 5 (12) ◽  
pp. 8895-8902 ◽  
Author(s):  
E.-E. Bendeif ◽  
A. Gansmuller ◽  
K.-Y. Hsieh ◽  
S. Pillet ◽  
Th. Woike ◽  
...  
Keyword(s):  
Distribution Function ◽  
Solid State ◽  
Solid State Nmr ◽  
Pair Distribution Function ◽  
Function Analysis ◽  
Structural Characterisation ◽  
Atomic Pair Distribution Function ◽  
X Ray Scattering ◽  
Atomic Pair

Total X-ray scattering coupled to atomic pair distribution function analysis (PDF) and solid state NMR allowed the identification and structural characterisation of isolated molecules and nanocrystals of sodium nitroprusside confined in mesoporous silica.

Solid-State NMR Structure Determination of Whole Anchoring Threads from the Blue Mussel Mytilus edulis

2012 ◽  
Vol 14 (1) ◽  
pp. 132-141 ◽  
Author(s):  
Alexandre A. Arnold ◽  
Frédéric Byette ◽  
Marc-Olivier Séguin-Heine ◽  
André LeBlanc ◽  
Lekha Sleno ◽  
...  
Keyword(s):  
Solid State ◽  
Mytilus Edulis ◽  
Structure Determination ◽  
Solid State Nmr ◽  
Blue Mussel ◽  
Nmr Structure ◽  
Nmr Structure Determination
Sign in / Sign up

Export Citation Format

Share Document