51V magic angle spinning solid state NMR studies of Bi4V2O11 in oxidized and reduced states

2000 ◽  
Vol 2 (19) ◽  
pp. 4477-4483 ◽  
Author(s):  
F. Delmaire ◽  
M. Rigole ◽  
E. A. Zhilinskaya ◽  
A. Aboukaı ◽  
R. Hubaut ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Nmr Studies ◽  
Angle Spinning

Solid-state NMR studies of cadmium: 113Cd1H cross polarization and magic-angle spinning

1980 ◽  
Vol 41 (1) ◽  
pp. 158-168 ◽  
Author(s):  
T.T.P Cheung ◽  
L.E Worthington ◽  
P.Dubois Murphy ◽  
B.C Gerstein
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Polarization ◽  
Nmr Studies ◽  
Angle Spinning

scholarly journals Strategies for RNA Resonance Assignment by 13C/15N- and 1H-Detected Solid-State NMR Spectroscopy

2021 ◽  
Vol 8 ◽  
Author(s):  
Philipp Innig Aguion ◽  
Alexander Marchanka
Keyword(s):  
Solid State ◽  
Resonance Assignment ◽  
Structure Determination ◽  
Solid State Nmr ◽  
Isotope Labeling ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Nmr Studies ◽  
Rna Resonance Assignment ◽  
Angle Spinning

Magic angle spinning (MAS) solid-state NMR (ssNMR) is an established tool that can be applied to non-soluble or non-crystalline biomolecules of any size or complexity. The ssNMR method advances rapidly due to technical improvements and the development of advanced isotope labeling schemes. While ssNMR has shown significant progress in structural studies of proteins, the number of RNA studies remains limited due to ssNMR methodology that is still underdeveloped. Resonance assignment is the most critical and limiting step in the structure determination protocol that defines the feasibility of NMR studies. In this review, we summarize the recent progress in RNA resonance assignment methods and approaches for secondary structure determination by ssNMR. We critically discuss advantages and limitations of conventional 13C- and 15N-detected experiments and novel 1H-detected methods, identify optimal regimes for RNA studies by ssNMR, and provide our view on future ssNMR studies of RNA in large RNP complexes.

scholarly journals Magic Angle Spinning Solid State NMR Studies of Oxidized Apolipoprotein A-I Aggregates

2018 ◽  
Vol 114 (3) ◽  
pp. 569a
Author(s):  
Jennifer C. Boatz ◽  
Gary Chan ◽  
Andrzej Witkowski ◽  
Patrick C.A. van der Wel ◽  
Giorgio Cavigiolio
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Nmr Studies ◽  
Apolipoprotein A ◽  
Angle Spinning

scholarly journals Combination of solid state NMR and DFT calculation to elucidate the state of sodium in hard carbon electrodes

2016 ◽  
Vol 4 (34) ◽  
pp. 13183-13193 ◽  
Author(s):  
Ryohei Morita ◽  
Kazuma Gotoh ◽  
Mika Fukunishi ◽  
Kei Kubota ◽  
Shinichi Komaba ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Dft Calculation ◽  
Magic Angle Spinning ◽  
The State ◽  
Mas Nmr ◽  
Magic Angle ◽  
Multiple Quantum ◽  
Hard Carbon ◽  
Angle Spinning

We examined the state of sodium electrochemically inserted in HC prepared at 700–2000 °C using solid state Na magic angle spinning (MAS) NMR and multiple quantum (MQ) MAS NMR.

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