Facile one-pot synthesis of 2-amino-1,3,4-oxadiazole tethered peptidomimetics by molecular-iodine-mediated cyclodeselenization

2017 ◽  
Vol 41 (19) ◽  
pp. 11225-11229 ◽  
Author(s):  
L. Santhosh ◽  
C. Srinivasulu ◽  
S. Durgamma ◽  
Girish Prabhu ◽  
Vommina V. Sureshbabu
Keyword(s):  
Molecular Iodine ◽  
One Pot ◽  
Highly Efficient ◽  
One Pot Synthesis

Mild and highly efficient I2 and Et3N aided cyclodeselenization of in situ generated selenosemicarbazide is described to obtain 2-amino-1,3,4-oxadiazole peptidomimetics.

ChemInform Abstract: Molecular Iodine in [bmim][BF4]: A Highly Efficient Green Catalytic System for One-Pot Synthesis of 1,3-Oxathiolan-5-one.

ChemInform ◽  
2011 ◽  
Vol 42 (8) ◽  
pp. no-no
Author(s):  
Manika Dewan ◽  
Ajeet Kumar ◽  
Amit Saxena ◽  
Arnab De ◽  
Subho Mozumdar
Keyword(s):  
Catalytic System ◽  
Molecular Iodine ◽  
One Pot ◽  
Highly Efficient ◽  
One Pot Synthesis

Molecular iodine in [bmim][BF4]: a highly efficient green catalytic system for one-pot synthesis of 1,3-oxathiolan-5-one

2010 ◽  
Vol 51 (47) ◽  
pp. 6108-6110 ◽  
Author(s):  
Manika Dewan ◽  
Ajeet Kumar ◽  
Amit Saxena ◽  
Arnab De ◽  
Subho Mozumdar
Keyword(s):  
Catalytic System ◽  
Molecular Iodine ◽  
One Pot ◽  
Highly Efficient ◽  
One Pot Synthesis

Highly Efficient, One-Pot, Solvent-Free Synthesis of Highly Substituted Imidazoles Using Molecular Iodine as Catalyst

2011 ◽  
Vol 396-398 ◽  
pp. 1871-1874
Author(s):  
Yi Ming Ren ◽  
Chun Cai
Keyword(s):  
Molecular Iodine ◽  
Solvent Free ◽  
One Pot ◽  
Product Yields ◽  
Highly Efficient ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Solvent Free Synthesis ◽  
Tetrasubstituted Imidazoles

Highly efficient, one-pot synthesis of 2,4,5-trisubstituted and 1,2,4,5-tetrasubstituted imidazoles under solvent-free conditions using molecular iodine as the catalyst is described with excellent product yields.

Ultrasound promoted green synthesis of benzofuran substituted thiazolo[3,2-b][1,2,4]triazoles

2017 ◽  
Vol 6 (1) ◽  
Author(s):  
Surender Kumar ◽  
Dinesh Kumar Sharma
Keyword(s):  
Green Synthesis ◽  
Molecular Iodine ◽  
One Pot ◽  
Highly Efficient ◽  
One Pot Synthesis ◽  
Ultrasonic Conditions

AbstractA highly efficient, eco-friendly and one-pot synthesis of benzofuran substituted thiazolo[3,2-b][1,2,4]triazoles was developed involving the reaction of 2-acetyl benzofurans and 5-mercapto-3-(4-chlorophenyl)-1,2,4triazole in the presence of molecular iodine under ultrasonic conditions to give 5-(benzofuran-2-yl)-acylthio-3-(4-chlorophenyl)-1,2,4triazoles, which was further cyclised using Eaton’s reagent under microwave conditions to give 5-(benzofuran-2-yl)-2-(4-chlorophenyl)thiazolo[3,2-b][1,2,4]triazoles.

scholarly journals “In Situ” Generated “HCl”: A Highly Efficient Catalyst for One-Pot Synthesis of 1H-Indazolo [1,2-b]phthalazine-1,6,11-triones and 1Hpyrazolo[1,2-b]phthalazine-5,10-diones under Solvent-Free Conditions

2017 ◽  
Vol 58 (2) ◽  
Author(s):  
Behrooz Maleki ◽  
Samaneh Sedigh Ashrafi
Keyword(s):  
Phthalic Anhydride ◽  
Solvent Free ◽  
Synthetic Route ◽  
Reaction Conditions ◽  
One Pot ◽  
Efficient Catalyst ◽  
Highly Efficient ◽  
One Pot Synthesis ◽  
Solvent Free Conditions

<p>The rapid and environmental synthetic route to produce 1<em>H</em>-indazolo[1,2-b] phthalazine-1,6,11-triones and 1<em>H</em>-pyrazolo[1,2-b]phthalazine-5,10-diones derivatives have been developed <em>via</em> multicomponent and one-pot reactions of various aldehydes, cyclic or acyclic 1,3-diketones with: <em>i)</em> phthalhydrazide or <em>ii)</em> phthalic anhydride-hydrazinium hydroxide using wet 2,4,6-trichlorotriazine (TCT) as catalyst under solvent-free conditions. Simple and mild reaction conditions, the use of a cheap catalyst and easy workup and isolation are notable features of this method.</p>

Indium Bromide-catalyzed Unprecedented Hydrogenolysis: A Novel One-Pot Synthesis of Per-O-Acetylated β-carboxymethyl O and S-glycosides

2020 ◽  
Vol 24 (8) ◽  
pp. 900-908
Author(s):  
Ram Naresh Yadav ◽  
Amrendra K Singh ◽  
Bimal Banik
Keyword(s):  
Asymmetric Synthesis ◽  
Chiral Auxiliary ◽  
Bioactive Molecules ◽  
One Pot ◽  
Enantiomerically Pure ◽  
Stereoselective Glycosylation ◽  
One Pot Synthesis ◽  
Wide Range

Numerous O (oxa)- and S (thia)-glycosyl esters and their analogous glycosyl acids have been accomplished through stereoselective glycosylation of various peracetylated bromo sugar with benzyl glycolate using InBr3 as a glycosyl promotor followed by in situ hydrogenolysis of resulting glycosyl ester. A tandem glycosylating and hydrogenolytic activity of InBr3 has been successfully investigated in a one-pot procedure. The resulting synthetically valuable and virtually unexplored class of β-CMGL (glycosyl acids) could serve as an excellent potential chiral auxiliary in the asymmetric synthesis of a wide range of enantiomerically pure medicinally prevalent β-lactams and other bioactive molecules of diverse medicinal interest.

Green and Highly Efficient One-Pot Synthesis of Some New Bis Thiazolidinones

2013 ◽  
Vol 10 (10) ◽  
pp. 764-769 ◽  
Author(s):  
Akbar Mobinikhaledi ◽  
Alireza Amiri
Keyword(s):  
One Pot ◽  
Highly Efficient ◽  
One Pot Synthesis

Fast and highly efficient one-pot synthesis of polyoxadiazole/carbon nanotube nanocomposites in mild acid

2010 ◽  
Vol 60 (3) ◽  
pp. 517-528 ◽  
Author(s):  
Marcio R Loos ◽  
Volker Abetz ◽  
Karl Schulte
Keyword(s):  
Carbon Nanotube ◽  
One Pot ◽  
Highly Efficient ◽  
One Pot Synthesis ◽  
Mild Acid

Hypervalent-Iodine Mediated One-Pot Synthesis of Isoxazolines and Isoxazoles bearing Difluoromethyl Phosphonate Moiety

2021 ◽  
Author(s):  
Romana Pajkert ◽  
Henryk Koroniak ◽  
Pawel Kafarski ◽  
Gerd Volker Roeschenthaler
Keyword(s):  
Nitrile Oxide ◽  
Dipolar Cycloaddition ◽  
Hypervalent Iodine ◽  
One Pot ◽  
One Pot Synthesis

A one-pot, regioselective 1,3-dipolar cycloaddition of in situ generated (diethoxyphosphoryl)difluoromethyl nitrile oxide toward selected alkenes and alkynes is reported. This protocol enables facile access to 3,5-disubstituted isoxazolines and isoxazoles bearing...

Sign in / Sign up

Export Citation Format

Share Document