scholarly journals In situ structural kinetics of picosecond laser-induced heating and fragmentation of colloidal gold spheres

2020 ◽  
Vol 22 (9) ◽  
pp. 4993-5001 ◽  
Author(s):  
Anna Rosa Ziefuss ◽  
Stefan Reich ◽  
Sven Reichenberger ◽  
Matteo Levantino ◽  
Anton Plech
Keyword(s):  
Colloidal Gold ◽  
Picosecond Laser ◽  
Time Resolved ◽  
Gold Colloids ◽  
X Ray ◽  
X Ray Scattering ◽  
Kinetics Of ◽  
Ray Scattering

The structural and energetic pathway of picosecond laser fragmentation of gold colloids has been clarified by time-resolved X-ray scattering.

In situ Time-Resolved Small-Angle X-ray Scattering Reveals the Formation Kinetics of Polyelectrolyte Complex Micelles

2019 ◽  
Author(s):  
Hao Wu ◽  
Jeffrey Ting ◽  
Siqi Meng ◽  
Matthew Tirrell
Keyword(s):  
Small Angle ◽  
Self Assembly ◽  
Electrostatic Interactions ◽  
Polyelectrolyte Complex ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Kinetics Of ◽  
Ray Scattering

We have directly observed the <i>in situ</i> self-assembly kinetics of polyelectrolyte complex (PEC) micelles by synchrotron time-resolved small-angle X-ray scattering, equipped with a stopped-flow device that provides millisecond temporal resolution. This work has elucidated one general kinetic pathway for the process of PEC micelle formation, which provides useful physical insights for increasing our fundamental understanding of complexation and self-assembly dynamics driven by electrostatic interactions that occur on ultrafast timescales.

scholarly journals Microfluidics for Time-Resolved Small-Angle X-Ray Scattering

2020 ◽  
Author(s):  
Susanne Seibt ◽  
Timothy Ryan
Keyword(s):  
Self Assembly ◽  
Structural Evolution ◽  
Time Resolved ◽  
X Ray ◽  
Structural Characterisation ◽  
X Ray Scattering ◽  
Saxs Analysis ◽  
Kinetics Of ◽  
Ray Scattering

With the advent of new in situ structural characterisation techniques including X-ray scattering, there has been an increased interest in investigations of the reaction kinetics of nucleation and growth of nanoparticles as well as self-assembly processes. In this chapter, we discuss the applications of microfluidic devices specifically developed for the investigation of time resolved analysis of growth kinetics and structural evolution of nanoparticles and nanofibers. We focus on the design considerations required for spectrometry and SAXS analysis, the advantages of using a combination of SAXS and microfluidics for these measurements, and discuss in an applied fashion the use of these devices for time-resolved research.

Time-Resolved Measurements of Overlayer Ordering in Electrodeposition

1996 ◽  
Vol 451 ◽  
Author(s):  
A. C. Finnefrock ◽  
L. J. Bullert ◽  
K. L. Ringland ◽  
P. D. Tingi ◽  
H. D. Abruña ◽  
...  
Keyword(s):  
Scattering Data ◽  
Electrode Position ◽  
Initial Value ◽  
Time Resolved ◽  
X Ray ◽  
Surface Ordering ◽  
X Ray Scattering ◽  
Kinetics Of ◽  
Ray Scattering

ABSTRACTWe report in situ time-resolved surface x-ray scattering measurements of the underpoten-tial deposition of Cu2+ on Pt(111) in the presence of Cl− in HClO4 solution. Chronoamperometric (current vs. time) measurements indicate that after a potential step, the electrode-position current decays to 1/e of its initial value in at most 0.12 seconds. In contrast, our simultaneous time-resolved surface x-ray scattering data reveal that the overlayer requires on the order of two seconds to develop long-range periodic order. These results demonstrate that the kinetics of surface ordering can be significantly different from the kinetics of charge-transfer and illustrate the power of time-resolved surface x-ray scattering for in situ studies of electrodeposition.

In Situ Wide- and Small-Angle X-ray Scattering Study of Melting Kinetics of Isotactic Poly(propylene)

2003 ◽  
Vol 36 (11) ◽  
pp. 4042-4050 ◽  
Author(s):  
Patrick S. Dai ◽  
Peggy Cebe ◽  
Malcolm Capel ◽  
Rufina G. Alamo ◽  
Leo Mandelkern
Keyword(s):  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Melting Kinetics ◽  
Scattering Study ◽  
Poly Propylene ◽  
Kinetics Of ◽  
Ray Scattering

scholarly journals In Situ Time-Resolved X-ray Scattering Study of Isotactic Polypropylene in Additive Manufacturing

2019 ◽  
Vol 11 (40) ◽  
pp. 37112-37120 ◽  
Author(s):  
Yuval Shmueli ◽  
Yu-Chung Lin ◽  
Sungsik Lee ◽  
Mikhail Zhernenkov ◽  
Rina Tannenbaum ◽  
...  
Keyword(s):  
Additive Manufacturing ◽  
Isotactic Polypropylene ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Scattering Study ◽  
Ray Scattering

D-94 Invited—In-Situ and Time Resolved Small-Angle X-ray Scattering

2010 ◽  
Vol 25 (2) ◽  
pp. 211-211
Author(s):  
B. G. Landes ◽  
B. J. Kern ◽  
T. J. Hermel-Davidock ◽  
M. Demirors ◽  
J. D. Weinhold ◽  
...  
Keyword(s):  
Small Angle ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Characterization of the Initial Stages of SBA-15 Synthesis by in Situ Time-Resolved Small-Angle X-ray Scattering

2005 ◽  
Vol 109 (48) ◽  
pp. 22780-22790 ◽  
Author(s):  
Andrei Y. Khodakov ◽  
Vladimir L. Zholobenko ◽  
Marianne Impéror-Clerc ◽  
Dominique Durand
Keyword(s):  
Small Angle ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering
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