Effect of Deep Cryogenic Treatment on the Carbide Precipitation and Tribological Behavior of D2 Steel

2007 ◽  
Vol 22 (4) ◽  
pp. 474-480 ◽  
Author(s):  
D. Das ◽  
A. K. Dutta ◽  
V. Toppo ◽  
K. K. Ray
Keyword(s):  
Tribological Behavior ◽  
Cryogenic Treatment ◽  
Carbide Precipitation ◽  
Deep Cryogenic Treatment ◽  
D2 Steel

Evaluation of Deep Criogenic Treatment at Microabrasive Wear of Aisi D2 Steel

2015 ◽  
Vol 1120-1121 ◽  
pp. 1257-1263
Author(s):  
Cosme Roberto Moreira Silva ◽  
Tiago F.O. Melo ◽  
José A. Araújo ◽  
J.L.A. Ferreira ◽  
S.J. Gobbi
Keyword(s):  
Wear Resistance ◽  
Treatment Cycle ◽  
Cryogenic Treatment ◽  
Deep Cryogenic Treatment ◽  
Abrasive Resistance ◽  
Austenitization Temperature ◽  
Aisi D2 Steel ◽  
X Ray ◽  
Aisi D2 ◽  
D2 Steel

Wear resistance of tool steels can be increased with deep cryogenic treatment (DCT) application. Mechanisms related to DCT are still not completely understood. Microabrasive wear resistance of cryogenically treated samples of AISI D2 steel was evaluated in terms of austenitization temperature at heat treatment cycle and quenching steps related to DCT. X-ray difractometry, scanning and optical microscopy and quantitative evaluation of carbides with image analysis were carried out aiming material characterization. For samples subjected to higher austenitization temperatures, the DCT treatment does not increase abrasive wear resistance. For samples treated at lower austenitization temperature, the DCT treatment results on 44% increase at abrasive resistance. This effect is correlated to the increase of the amount of fine carbides distributed at samples matrices cryogenically treated.

The Influence of Post-Quenching Deep Cryogenic Treatment on Tempering Processes and Properties of D2 Tool Steel. Studies of Structure, XRD, Dilatometry, Hardness and Fracture Toughness

2006 ◽  
Vol 258-260 ◽  
pp. 415-420 ◽  
Author(s):  
Ignacy Wierszyłłowski
Keyword(s):  
Fracture Toughness ◽  
Cryogenic Treatment ◽  
Cryogenic Temperatures ◽  
Deep Cryogenic Treatment ◽  
Treated Steel ◽  
The Matrix ◽  
Xrd Studies ◽  
Number Of Publications ◽  
D2 Steel ◽  
Tetragonal Martensite

A significant increase in durability of cryogenically treated tools after quenching was reported by a number of publications [1, 2]. As research studies show [4, 5, 6, 7], the main reason for this is the kind of carbides precipitated during tempering at temperature range of 150 –200 0C, which is different than in the case of conventional treatment. These carbides are finer and more evenly distributed in the matrix of steel. The number of carbides is higher than in conventionally treated steels because of higher fraction of martensite in cryogenically treated steels produced by retained austenite transformation at cooling to deep cryogenic temperatures. The number of carbides precipitated from martensite at low temperatures of tempering is proportional to shrinkage produced at the same temperatures of tempering. Calculations on the basis of dilatometric experiments show that the shrinkage difference between the same D2 steel cryogenically and conventionally treated is higher than that which results from the increased fraction of martensite in cryogenically treated steel. The XRD studies of cryogenically treated steel show a presence of two kinds of martensites differing in tetragonality. Low temperature tempering of cryogenically treated steel produced two types of carbides – ε carbide and η carbide. The conventionally treated steel consists of one kind of tetragonal martensite and one kind of carbide - the ε carbide. The hardness of cryogenically treated samples was somewhat higher than in conventionally treated ones, while fracture toughness of conventionally treated samples was somewhat higher than in cryogenically treated ones. The results obtained were discussed in reference to literature data.

scholarly journals Effectiveness of deep cryogenic treatment on carbide precipitation

2020 ◽  
Vol 9 (6) ◽  
pp. 13014-13026 ◽  
Author(s):  
Patricia Jovičević-Klug ◽  
Matic Jovičević-Klug ◽  
Bojan Podgornik
Keyword(s):  
Cryogenic Treatment ◽  
Carbide Precipitation ◽  
Deep Cryogenic Treatment

Structure-Property Correlation of Cryotreated AISI D2 Steel

2010 ◽  
Vol 117 ◽  
pp. 49-54 ◽  
Author(s):  
Debdulal Das ◽  
Apurba Kishore Dutta ◽  
Kalyan Kumar Ray
Keyword(s):  
Wear Resistance ◽  
Cryogenic Treatment ◽  
Structure Property ◽  
Tool Steels ◽  
Deep Cryogenic Treatment ◽  
Aisi D2 Steel ◽  
Secondary Carbides ◽  
Varied Degree ◽  
Aisi D2 ◽  
D2 Steel

This study aims to reveal the underlying mechanism associated with the enhancement of wear resistance of tool steels by deep cryogenic treatment and to resolve the issue of reported varied degree of improvement in wear resistance through structure-property correlation of cryotreated vis-à-vis conventionally treated AISI D2 steel. Microstructures of heat treated specimens have been characterized employing various techniques with specific emphasis on quantitative estimation of the characteristics of secondary carbides. Evaluations of properties include measurements of bulk hardness, apparent strength of the matrix, fracture toughness and dry sliding wear resistance under wide rage of normal loads supplemented by in-depth characterizations of worn surfaces, wear debris and subsurfaces of worn specimens in order to identify the operative mode and mechanism of wear. It has been demonstrated that the favorable modifications of the precipitation behavior of secondary carbides in addition to removal of retained austenite are the governing mechanisms for the enhancement of wear resistance of tool steels by deep cryogenic treatment. The cause of the reported varied degree of improvement in wear resistance by deep cryogenic treatment has been explained by disparity of the operative modes and mechanisms of wear.

Carbide Precipitation During Tempering of a Tool Steel Subjected to Deep Cryogenic Treatment

2014 ◽  
Vol 45 (5) ◽  
pp. 2453-2465 ◽  
Author(s):  
V. G. Gavriljuk ◽  
V. A. Sirosh ◽  
Yu. N. Petrov ◽  
A. I. Tyshchenko ◽  
W. Theisen ◽  
...  
Keyword(s):  
Tool Steel ◽  
Cryogenic Treatment ◽  
Carbide Precipitation ◽  
Deep Cryogenic Treatment

Effect of Deep Cryogenic Treatment on Carbide Precipitation and Mechanical Properties of Tool Steel

2006 ◽  
Vol 118 ◽  
pp. 9-14 ◽  
Author(s):  
Young Mok Rhyim ◽  
Sang Ho Han ◽  
Young Sang Na ◽  
Jong Hoon Lee
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Tool Steel ◽  
Retained Austenite ◽  
Cryogenic Treatment ◽  
Carbide Precipitation ◽  
Deep Cryogenic Treatment ◽  
Tempering Temperature ◽  
Fine Carbide ◽  
Forming Temperature

It is well known that the durability of tool steel could be improved by deep cryogenic treatment. It has been assumed that the increase of service life of tool steel caused by decrease of retained austenite and/or by formation of nano-scale fine η-carbide. But the principles of deep cryogenic treatment remain unclear yet. In this research, to manifest the effect of deep cryogenic treatment on wear resistance, the specimen was emerged in liquid nitrogen for 20 hours for deep cryogenic treatment after austenitizing and the following tempering temperature was varied. The microstructure of specimens was observed using TEM and the mechanical properties and wear resistance were examined. As the tempering temperature increased, the carbides became larger and fine carbides were formed above certain temperature. In the case of deep cryogenic treated specimen, the number of carbides increased while the carbides size was decreased, furthermore, the fine carbide forming temperature was lowered also. It was considered that the deep cryogenic treatment increased the driving force for the nucleation of carbides. As tempering temperature increased, hardness decreased while wear resistance and impact energy increased. The deep cryogenic treated specimens showed this tendency more clearly. It was considered that the wear resistance is affected not only to the hardness but also to the precipitation of fine carbides, and this carbide evolution can be optimized through the deep cryogenic treatment.

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