X-ray diffraction study on the amorphization of the Pd80Si20 powder mixture by mechanical alloying

1993 ◽  
Vol 68 (6) ◽  
pp. 833-844 ◽  
Author(s):  
S. Martelli ◽  
W. Guo ◽  
M. Magini ◽  
F. Padella ◽  
D. Zedda
2012 ◽  
Vol 05 ◽  
pp. 581-588
Author(s):  
ROUHOLLAH YAZDI ◽  
SEYED FAESHID KASHANI-BOZORG

In this investigation, TiN / TiB 2/ TiAl nano-composite powder was produced by mechanical alloying technique and subsequent heat treatment. A powder mixture of Ti , BN , and Al with a molar ratio of 4:2:1 was milled for up to 70 h. Microstructures were studied and characterized using X-ray diffraction, scanning electron microscopy and energy-dispersive spectroscopy. The results indicated that TiN and TiB 2-based phases were formed in an amorphous Ti ( Al ) matrix after 30 h of ball milling. With progression of the milling, the amorphous Ti ( Al ) solid solution is partially crystallized and the particle size reduced significantly. Subsequent annealing of the milled product at 600 °C for 0.5 h resulted in the transformation of the unstable amorphous Ti ( Al ) to TiAl crystal structure and formation of TiN / TiB 2/ TiAl nano-composite powder.


1997 ◽  
Vol 260 (1-2) ◽  
pp. 135-138 ◽  
Author(s):  
I. Apachitei ◽  
L.M. Craus ◽  
Gh. Calugaru

1986 ◽  
Vol 47 (1) ◽  
pp. 133-138 ◽  
Author(s):  
D. Guillon ◽  
A. Skoulios ◽  
J.J. Benattar

1987 ◽  
Vol 48 (8) ◽  
pp. 1357-1361 ◽  
Author(s):  
F. Dénoyer ◽  
G. Heger ◽  
M. Lambert ◽  
J.M. Lang ◽  
P. Sainfort

1980 ◽  
Vol 41 (C1) ◽  
pp. C1-145-C1-146 ◽  
Author(s):  
B. Greenberg ◽  
G. M. Rothberg

2019 ◽  
Vol 107 (2) ◽  
pp. 207 ◽  
Author(s):  
Jaroslav Čech ◽  
Petr Haušild ◽  
Miroslav Karlík ◽  
Veronika Kadlecová ◽  
Jiří Čapek ◽  
...  

FeAl20Si20 (wt.%) powders prepared by mechanical alloying from different initial feedstock materials (Fe, Al, Si, FeAl27) were investigated in this study. Scanning electron microscopy, X-ray diffraction and nanoindentation techniques were used to analyze microstructure, phase composition and mechanical properties (hardness and Young’s modulus). Finite element model was developed to account for the decrease in measured values of mechanical properties of powder particles with increasing penetration depth caused by surrounding soft resin used for embedding powder particles. Progressive homogenization of the powders’ microstructure and an increase of hardness and Young’s modulus with milling time were observed and the time for complete homogenization was estimated.


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