Mesomorphic properties, microwave-assisted synthesis, and antimicrobial evaluation of novel Schiff base functionalized resorcin[4]arene derivatives

2021 ◽  
Vol 715 (1) ◽  
pp. 37-55
Author(s):  
Jinal A. Gajjar ◽  
Rajesh H. Vekariya ◽  
Vinay S. Sharma ◽  
Seema N. Kher ◽  
Dhanji P. Rajani ◽  
...  
Keyword(s):  
Schiff Base ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Antimicrobial Evaluation ◽  
Mesomorphic Properties

scholarly journals One-Pot Microwave-Assisted Synthesis of Water-Soluble Pyran-2,4,5-triol Glucose Amine Schiff Base Derivative: XRD/HSA Interactions, Crystal Structure, Spectral, Thermal and a DFT/TD-DFT

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 117
Author(s):  
Yousef Hijji ◽  
Rajeesha Rajan ◽  
Hamdi Ben Yahia ◽  
Said Mansour ◽  
Abdelkader Zarrouk ◽  
...  
Keyword(s):  
Schiff Base ◽  
Molecular Orbital ◽  
Density Functional ◽  
Condensation Reaction ◽  
3D Structure ◽  
Water Soluble ◽  
Microwave Assisted Synthesis ◽  
One Pot ◽  
Microwave Assisted ◽  
Td Dft

The(3R,4R,6R)-3-(((E)-2-hydroxybenzylidene)amino)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,4,5-triol water-soluble Glucose amine Schiff base (GASB-1) product was made available by condensation of 2-hydroxybenzaldehyde with (3R,6R)-3-amino-6-(hydroxymethyl)-tetra-hydro-2H-pyran-2,4,5-triol under mono-mode microwave heating. A one-pot 5-minute microwave-assisted reaction was required to complete the condensation reaction with 90% yield and without having byproducts. The 3D structure of GASB-1 was solved from single crystal X-ray diffraction data and computed by DFT/6-311G(d,p). The Hirshfeld surface analysis (HSA), molecular electronic potential (MEP), Mulliken atomic charge (MAC), and natural population analysis (NPA) were performed. The IR and UV-Vis spectra were matched to their density functional theory (DFT) relatives and the thermal behavior was resolved in an open-room condition via thermogravimetry/Derivative thermogravimetry (TG/DTG) and differential scanning calorimetry (DSC). The highest occupied molecular orbital/lowest unoccupied molecular orbital (HOMO/LUMO), density of state (DOS), and time-dependence TD-DFT computations were correlated to the experimental electron transfer in water and acrylonitrile solvents.

Microwave‐Assisted Synthesis, Antioxidant, and Antimicrobial Evaluation of Piperazine‐Azole‐Fluoroquinolone Based 1,2,4‐Triazole Derivatives

2018 ◽  
Vol 55 (12) ◽  
pp. 2744-2759 ◽  
Author(s):  
Serap Basoglu Ozdemir ◽  
Neslihan Demirbas ◽  
Ahmet Demirbas ◽  
Faik Ahmet Ayaz ◽  
Nesrin Çolak
Keyword(s):  
Microwave Assisted Synthesis ◽  
Triazole Derivatives ◽  
Microwave Assisted ◽  
Antimicrobial Evaluation

scholarly journals Microwave Assisted Synthesis and Antimicrobial Evaluation of Schiff Bases of Indole-3-aldehyde

2011 ◽  
Vol 8 (1) ◽  
pp. 305-311 ◽  
Author(s):  
Priyanka Kamaria ◽  
N. Kawathekar ◽  
Prerna Chaturvedi
Keyword(s):  
Schiff Bases ◽  
Antimicrobial Agents ◽  
Microwave Assisted Synthesis ◽  
Bacterial Strains ◽  
Mass Spectral Analysis ◽  
Gram Positive ◽  
Gram Negative ◽  
Mass Spectral ◽  
Microwave Assisted ◽  
Antimicrobial Evaluation

In order to develop new antimicrobial agents, a series of Schiff bases of indole-3-aldehyde were synthesized by microwave assisted synthesis by takingDMFas solvent and evaluated for their antimicrobial activity. All the synthesized compounds were characterized byIR,1HNMRand mass spectral analysis. All compounds were tested against five gram positive and five gram negative bacterial strains and one fungal strain. All compounds exhibited better activity against gram positive strains than against gram negative strains and the compounds were found more active againstS.aureusandB.subtilis.

Microwave-assisted synthesis of 1,3,4-thiadiazole Schiff base derivatives

2011 ◽  
Vol 35 (8) ◽  
pp. 442-443 ◽  
Author(s):  
Jun Hu ◽  
Jianguang Sun ◽  
Taoyu Zhou ◽  
Yanhua Xu
Keyword(s):  
Schiff Base ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Schiff Base Derivatives
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