scholarly journals Determination of volatile fatty acids in tofu wastewater by capillary gas chromatography with flame ionization detection: A Comparison of extraction methods

Author(s):  
R T Rosmalina ◽  
Widyarani ◽  
U Hamidah ◽  
N Sintawardani
2016 ◽  
Vol 39 (22) ◽  
pp. 4377-4383 ◽  
Author(s):  
Roman Kanďár ◽  
Petra Drábková ◽  
Lenka Andrlová ◽  
Adam Kostelník ◽  
Alexander Čegan

2011 ◽  
Vol 63 (12) ◽  
pp. 2873-2877 ◽  
Author(s):  
Anna Banel ◽  
Marta Wasielewska ◽  
Monika Felchner-Żwirełło ◽  
Bogdan Zygmunt

In order to determine volatile fatty acids (short chain monocarboxylic acids with 2 to 6 carbon atoms in a molecule) in leachates formed in organic waste piles a procedure based on static headspace (HS) coupled with gas chromatography (GC) have been proposed and optimized. The conditions of HS extraction and sample introduction into a gas chromatograph as well as of chromatographic separation were considered. Using flame ionization detection LODs were of the order of 0.02– 0.37 mg/L. The analyzed leachate collecting on and close to a zoo organic waste pile contained VFAs (Volatile Fatty Acids) at a concentration ranging from 5.5 mg/L to 0.88 g/L and from below LOD to 10.1 mg/L for pool water at some distance from the pile, respectively.


1996 ◽  
Vol 79 (3) ◽  
pp. 724-737 ◽  
Author(s):  
Nicholas H Low

Abstract A method using capillary gas chromatography with flame ionization detection was developed to determine the addition of high�fructose syrup and beet or cane invert syrup to apple or orange juice. Fingerprint oligosaccharides in these inexpensive sweeteners were not detectable (area < 1000) in pure apple or orange juice. One hundred twenty- three pure apple juice and 60 pure orange juice samples representing growing regions around the world were analyzed. Ten samples were intentionally adulterated with each sweetener at levels of 5, 10, and 15%. The detection limit for each sweetener was 5%.


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