Comparison Between Absolute Orientation Determination Methods of Doubly Rotated Blanks

Author(s):  
T. Garnier ◽  
J. Imbaud ◽  
X. Vacheret ◽  
E. Andrey ◽  
F. Sthal ◽  
...  
Crystals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 375 ◽  
Author(s):  
Yucheng Lan ◽  
Mobolaji Zondode ◽  
Hua Deng ◽  
Jia-An Yan ◽  
Marieme Ndaw ◽  
...  

Graphene is a kind of typical two-dimensional material consisting of pure carbon element. The unique material shows many interesting properties which are dependent on crystallographic orientations. Therefore, it is critical to determine their crystallographic orientations when their orientation-dependent properties are investigated. Raman spectroscopy has been developed recently to determine crystallographic orientations of two-dimensional materials and has become one of the most powerful tools to characterize graphene nondestructively. This paper summarizes basic aspects of Raman spectroscopy in crystallographic orientation of graphene nanosheets, determination principles, the determination methods, and the latest achievements in the related studies.


Author(s):  
H. Weiland ◽  
D. P. Field

Recent advances in the automatic indexing of backscatter Kikuchi diffraction patterns on the scanning electron microscope (SEM) has resulted in the development of a new type of microscopy. The ability to obtain statistically relevant information on the spatial distribution of crystallite orientations is giving rise to new insight into polycrystalline microstructures and their relation to materials properties. A limitation of the technique in the SEM is that the spatial resolution of the measurement is restricted by the relatively large size of the electron beam in relation to various microstructural features. Typically the spatial resolution in the SEM is limited to about half a micron or greater. Heavily worked structures exhibit microstructural features much finer than this and require resolution on the order of nanometers for accurate characterization. Transmission electron microscope (TEM) techniques offer sufficient resolution to investigate heavily worked crystalline materials.Crystal lattice orientation determination from Kikuchi diffraction patterns in the TEM (Figure 1) requires knowledge of the relative positions of at least three non-parallel Kikuchi line pairs in relation to the crystallite and the electron beam.


2019 ◽  
Vol 56 (1) ◽  
pp. 22-33
Author(s):  
U. Mühle ◽  
M. Löffler ◽  
T. Schubert ◽  
T. E. M. Staab ◽  
R. Krause-Rehberg ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document