Headspace gas chromatographic determination of 1,4-dioxane with adsorption preconcentration on silica modified with λ-carrageenan

2017 ◽  
Vol 72 (3) ◽  
pp. 295-302
Author(s):  
O. I. Fedorchuk ◽  
N. G. Kobylinska ◽  
V. N. Zaitsev
Keyword(s):  
Chromatographic Determination ◽  
Adsorption Preconcentration ◽  
Headspace Gas

Headspace gas chromatographic determination of ethylene oxide in air

1986 ◽  
Vol 21 (12) ◽  
pp. 701-704 ◽  
Author(s):  
R. Binetti ◽  
S. Di Marzio ◽  
P. Di Prospero ◽  
L. Gramiccioni ◽  
G. Viviano ◽  
...  
Keyword(s):  
Ethylene Oxide ◽  
Chromatographic Determination ◽  
Headspace Gas

Headspace gas-chromatographic determination of formaldehyde in urine

2017 ◽  
Vol 72 (1) ◽  
pp. 83-86 ◽  
Author(s):  
A. N. Alekseenko ◽  
O. M. Zhurba ◽  
N. V. Efimova ◽  
V. S. Rukavishnikov
Keyword(s):  
Chromatographic Determination ◽  
Headspace Gas

scholarly journals Headspace Gas Chromatographic Determination of 1,3-Butadiene in Simulated Saliva

2000 ◽  
Vol 83 (4) ◽  
pp. 929-932 ◽  
Author(s):  
Shirley Abrantes ◽  
Tereza C Dos Santos ◽  
Grazieli SimÕES
Keyword(s):  
Limit Of Detection ◽  
Chromatographic Determination ◽  
Calibration Graph ◽  
Chewing Gum ◽  
Preliminary Assessment ◽  
Headspace Gas ◽  
Sensitive Determination ◽  
Headspace Gc ◽  
Migration Limit

Abstract A headspace gas chromatographic (GC) method was developed to determine 1,3-butadiene (1,3-BD) in simulated saliva in contact with chewing gum. The calibration graph was linear, and the limit of detection was 0.004 mg/L, which is well below the migration limit for this substance. The headspace GC method provides rapid and reliable analysis for monitoring 1,3-BD migration from chewing gum into simulated saliva. In this paper, we report headspace methodology for sensitive determination of 1,3-BD in chewing gum and results of selected analyses, enabling preliminary assessment of possible exposure to 1,3-BD through migration.

Manual Headspace Gas-Solid Chromatographic Determination of Sub-Parts per Trillion Levels of Acrylonitrile in 3% Acetic Acid

1982 ◽  
Vol 65 (1) ◽  
pp. 184-187
Author(s):  
Timothy McNeal ◽  
Charles V Breder
Keyword(s):  
Acetic Acid ◽  
Detection Limit ◽  
Vapor Phase ◽  
Chromatographic Determination ◽  
Headspace Sampling ◽  
Carbonated Beverages ◽  
Headspace Gas ◽  
Detector Output ◽  
Output Amplifier

Abstract A procedure was developed for determining acrylonitrile (AN) in 3% acetic acid, the solvent used to simulate carbonated beverages. Manual headspace sampling, a detector output amplifier/filter, and vapor phase enhancement using an ionic material were combined to give a detection limit in the low parts per trillion range. AN standards were analyzed using the method, and the results are presented.

Sign in / Sign up

Export Citation Format

Share Document