Synthesis of Nanocrystalline Titanium Diboride in a Hypervelocity Plasma Jet

The present work reported a novel way of making nanocrystalline Ti-B phases (titanium boride and titanium diboride) in a hypersonic plasma jet. According to the purpose to synthesize nanosized Ti-B phases, experiments with different mass proportions of precursors were implemented. The optimal ratio of precursors, which leads to the yield of titanium diboride is 93.2% and the average particle size, doesn`t exceed 56.1 nm, is the ratio of Ti: B of 26.7: 73.3.

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A Mild Solvothermal Route to Nanocrystalline Titanium Diboride.

ChemInform ◽

10.1002/chin.200344208 ◽

2003 ◽

Vol 34 (44) ◽

Author(s):

Yunle Gu ◽

Yitai Qian ◽

Luyang Chen ◽

Fu Zhou

Keyword(s):

Titanium Diboride ◽

Solvothermal Route ◽

Nanocrystalline Titanium

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A reduction–boronation route to nanocrystalline titanium diboride

Solid State Communications ◽

10.1016/j.ssc.2004.01.037 ◽

2004 ◽

Vol 130 (3-4) ◽

pp. 231-233 ◽

Cited By ~ 11

Author(s):

Luyang Chen ◽

Yunle Gu ◽

Liang Shi ◽

Zeheng Yang ◽

Jianhua Ma ◽

...

Keyword(s):

Titanium Diboride ◽

Nanocrystalline Titanium

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A mild solvothermal route to nanocrystalline titanium diboride

Journal of Alloys and Compounds ◽

10.1016/s0925-8388(02)01173-8 ◽

2003 ◽

Vol 352 (1-2) ◽

pp. 325-327 ◽

Cited By ~ 43

Author(s):

Yunle Gu ◽

Yitai Qian ◽

Luyang Chen ◽

Fu Zhou

Keyword(s):

Titanium Diboride ◽

Solvothermal Route ◽

Nanocrystalline Titanium

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Tough ceramics by microwave sintering of nanocrystalline titanium diboride ceramics

Ceramics International ◽

10.1016/j.ceramint.2013.07.010 ◽

2014 ◽

Vol 40 (1) ◽

pp. 1303-1310 ◽

Cited By ~ 35

Author(s):

D. Demirskyi ◽

D. Agrawal ◽

A. Ragulya

Keyword(s):

Titanium Diboride ◽

Microwave Sintering ◽

Nanocrystalline Titanium

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Синтез нанокристаллического диборида титана в гиперскоростной плазменной струе

Письма в журнал технической физики ◽

10.21883/pjtf.2018.07.45886.17044 ◽

2018 ◽

Vol 44 (7) ◽

pp. 61

Author(s):

А.А. Сивков ◽

Д.Ю. Герасимов ◽

Д.С. Никитин

Keyword(s):

Titanium Diboride ◽

Experimental Investigations ◽

High Current ◽

Nanocrystalline Titanium ◽

Coaxial Magnetoplasma Accelerator

AbstractResults of experimental investigations of directly synthesizing nanocrystalline titanium diboride in a hypervelocity jet of electrodischarge plasma generated by a pulse high-current coaxial magnetoplasma accelerator with titanium electrodes are presented. The main result of the investigations is manufacturing a product with a mass of up to ∼3 g containing more than 90% of titanium diboride obtained mostly in the form of hexagonal and dodecagonal particles.

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