Determination of cobalt oxide activity in the La2O3-SrO-CoO system using high-temperature mass spectrometry

2014 ◽  
Vol 40 (3) ◽  
pp. 329-332 ◽  
Author(s):  
S. I. Lopatin ◽  
N. P. Bobrysheva ◽  
A. A. Selyutin
Keyword(s):  
Mass Spectrometry ◽  
High Temperature ◽  
Cobalt Oxide ◽  
High Temperature Mass Spectrometry

Vaporization and thermodynamics of the Cs 2 O‐MoO 3 system studied by high temperature mass spectrometry

2021 ◽  
Author(s):  
Valentina L. Stolyarova ◽  
Viktor A. Vorozhtcov ◽  
Sergey I. Lopatin ◽  
Sergey M. Shugurov ◽  
Elizaveta P. Simonenko ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
High Temperature ◽  
High Temperature Mass Spectrometry

scholarly journals Development, Optimization and Validation of a Sustainable and Quantifiable Methodology for the Determination of 2,4,6-Trichloroanisole, 2,3,4,6-Tetrachloroanisole, 2,4,6-Tribromoanisole, Pentachloroanisole, 2-Methylisoborneole and Geosmin in Air

Processes ◽  
2021 ◽  
Vol 9 (9) ◽  
pp. 1571
Author(s):  
Patricia Jové ◽  
Marina Vives-Mestres ◽  
Raquel De Nadal ◽  
Maria Verdum
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
High Temperature ◽  
Thermal Desorption ◽  
Mass Spectrometric ◽  
Gas Chromatography Mass Spectrometry ◽  
Air Analysis ◽  
Good Linearity ◽  
Repeatability And Reproducibility

Compounds 2,4,6-trichloroanisole (TCA), 2,3,4,6-tetrachloroanisole (TeCA), 2,4,6-tribromoanisole (TBA) and pentachloroanisole (PCA), 2-methylisoborneol (2MIB) and geosmin (GSM) have been reported as being responsible for cork and wine taint. A sustainable method based on thermal desorption-gas chromatography–mass spectrometry (TD-GC/MS) has been developed and optimized, taking into account desorption parameters and chromatographic and mass spectrometric conditions. The combination of parameters that jointly maximized the compound detection was as follows: desorption temperature at 300 °C, desorption time at 30 min, cryo-temperature at 20 °C and trap high temperature at 305 °C. The proposed methodology showed a good linearity (R ≤ 0.994) within the tested range (from 0.1 to 2 ng) for all target compounds. The precision expressed as repeatability and reproducibility was RSD < 10% in both. The limits of quantification ranged from 0.05 to 0.1 ng. The developed methodology and the sampling rates (R-values) of all targeted compounds (from 0.013 to 0.071 m3 h−1) were applied to the air analysis of two wineries. The results showed that the developed methodology is a sustainable and useful tool for the determination of these compounds in air.

scholarly journals Hydrogen Atmosphere Effect on Vaporization of Li2TiO3 by means of High Temperature Mass Spectrometry.

2003 ◽  
Vol 51 (1) ◽  
pp. 163-167 ◽  
Author(s):  
Tsuyoshi HOSHINO ◽  
Masaru YASUMOTO ◽  
Yoichi TAKAHASHI ◽  
Takayuki TERAI ◽  
Michio YAMAWAKI
Keyword(s):  
Mass Spectrometry ◽  
High Temperature ◽  
Hydrogen Atmosphere ◽  
Atmosphere Effect ◽  
High Temperature Mass Spectrometry
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