scholarly journals Texture Analysis of a Zinc Layer on a Steel Substrate Using Neutron Diffraction

1993 ◽  
Vol 21 (2-3) ◽  
pp. 71-78
Author(s):  
H.-G. Brokmeier

This paper describes the application of neutron diffraction to investigate the texture of a zinc layer 8 μm in thickness. In a nondestructive way both the texture of the zinc layer as well as the texture of the steel substrate were studied. Therefore, pole figures of iron ((110), (200) and (211)) and of zinc ((0002), (101¯0), (101¯1); and (101¯3)/(112¯0)) were measured; additionally the orientation distribution function of iron and zinc were calculated.

1995 ◽  
Vol 28 (5) ◽  
pp. 532-533 ◽  
Author(s):  
L.-G. Yu ◽  
H. Guo ◽  
B. C. Hendrix ◽  
K.-W. Xu ◽  
J.-W. He

A new simple method is proposed for determining the orientation distribution function (ODF) for three-dimensional texture analysis in a polycrystal based on the reality that the accuracy of an ODF is dependent on both the accuracy of each measured pole figure and the number of pole figures.


1995 ◽  
Vol 28 (5) ◽  
pp. 582-589 ◽  
Author(s):  
T. Baudin ◽  
J. Jura ◽  
R. Penelle ◽  
J. Pospiech

The calculation of characteristics describing texture as well as relations between orientations and morphological features of microstructure are based on single orientation measurements. For such experimental data, it is essential to estimate the number of necessary measurements of single orientations for a statistically significant representation of the investigated quantity, which, in the present paper, is the orientation distribution function (ODF). In a previous article [Pospiech, Jura & Gottstein (1993) Mater Sci. Forum, 157–162, 407–412], this number has been estimated by a criterion that is used here for a cubic and a hexagonal material. This approach is very useful since it allows one to estimate the minimum orientation number with or without referring to an ODF calculated from pole figures measured by X-ray or neutron diffraction.


1985 ◽  
Vol 29 ◽  
pp. 443-449
Author(s):  
Munetsugu Matsuo ◽  
Koichi Kawasaki ◽  
Tetsuya Sugai

AbstractAs a means for quantitative texture analysis, the crystallite orientation distribution function analysis has an important drawback: to bring ghosts as a consequence of the presence of a non-trivial kernel which consists of the spherical harmonics of odd order terms. In the spherical hamonic analysis, ghosts occur in the particular orientations by symmetry operation from the real orientation in accordance with the symmetry of the harmonics of even orders. For recovery of the odd order harmonics, the 9th-order generalized spherical harmonics are linearly combined and added to the orientation distribution function reconstructed from pole figures to a composite function. The coefficients of the linear combination are optimized to minimize the sum of negative values in the composite function. Reproducibility was simulated by using artificial pole figures of single or multiple component textures. Elimination of the ghosts is accompanied by increase in the height of real peak in the composite function of a single preferred orientation. Relative fractions of both major and minor textural components are reproduced with satisfactory fidelity In the simulation for analysis of multi-component textures.


2005 ◽  
Vol 495-497 ◽  
pp. 983-988
Author(s):  
N.Yu. Ermakova ◽  
Nikolay Y. Zolotorevsky ◽  
Yuri Titovets

The method is described which enables to determine the microtexture that is the orientation distribution within individual grains of a polycrystal. The microtexture is evaluated on the base of X-ray pole distributions measured for separate reflections, referred to as microscopic pole figures (MPF). The procedure for treatment of experimental MPF and the following computation of orientation distribution function is described in detail. Precision of the microtexture evaluation and possible ways of its improvement are discussed. As an example of the method application, orientation distribution within a single grain of aluminum polycrystal deformed by uniaxial compression up to 50% has been examined.


Texture ◽  
1972 ◽  
Vol 1 (1) ◽  
pp. 9-16 ◽  
Author(s):  
W. R. Krigbaum ◽  
Anna Marie Harkins Vasek

A test of the refinement procedure for improving the crystallite orientation distribution function is presented for a fiber texture sample of polyethylene terephthalate. This is a particularly difficult example because the triclinic unit cell offers no simplification due to symmetry, and the pole figures are sharply peaked. The analysis employed 17 observed pole figures and an additional 29 unobserved pole figures reconstructed from the crystallite orientation distribution function. After three cycles of refinement, in which the maximum value of the coefficient was increased from 6 to 16, the standard deviations, σq and σw, of the plane-normal and crystallite orientation distributions were reduced by about a factor of 3. The refined crystallite orientation distribution function indicates that the c-axis tends to align along the fiber axis for this polyethylene terephthalate sample.


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