Die 1H-NMR-spektroskopische Untersuchung der Struktur der dimeren 1.3-Dimethyluracile1 / Structure Determination of Dimeric 1,3-Dimethyl-Uracils by 1H-NMR-Spectroscopy

1972 ◽  
Vol 27 (12) ◽  
pp. 1481-1484 ◽  
Author(s):  
Egon Fahr ◽  
Peter Maul ◽  
Karl-Adolf Lehner ◽  
Dieter Scheutzow
Keyword(s):  
Nmr Spectroscopy ◽  
1H Nmr ◽  
Structure Determination ◽  
1H Nmr Spectroscopy ◽  
Nmr Spectra

Structures of dimeric dimethyl-uracils have been established by simulation of 90 Mc NMR spectra

scholarly journals Structure determination of the glycans of human-serum alpha1-antichymotrypsin using 1H-NMR spectroscopy and deglycosylation by N-glycanase

1991 ◽  
Vol 197 (1) ◽  
pp. 209-215 ◽  
Author(s):  
Anne LAINE ◽  
Eric HACHULLA ◽  
Gerard STRECKER ◽  
Jean-Claude MICHALSKI ◽  
Jean-Michel WIERUSZESKI
Keyword(s):  
Nmr Spectroscopy ◽  
Human Serum ◽  
1H Nmr ◽  
Structure Determination ◽  
1H Nmr Spectroscopy

scholarly journals Structure determination of oligosaccharides isolated from Cad erythrocyte membranes by permethylation analysis and 500-MHz 1H-NMR spectroscopy

1985 ◽  
Vol 146 (1) ◽  
pp. 125-129 ◽  
Author(s):  
Francoise HERKT ◽  
Jose Paz PARENTE ◽  
Yves LEROY ◽  
Bernard FOURNET ◽  
Dominique BLANCHARD ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
1H Nmr ◽  
Structure Determination ◽  
1H Nmr Spectroscopy ◽  
Erythrocyte Membranes

1H—NMR-spektroskopische Bestimmung der diastereomeren Reinheit und der absoluten Konfiguration am Phosphoratom von tButyl-phenyl-phosphinsäure-(—)-menthylester / Determination of the Diastereomeric Purity and the Absolute Configuration at Phosphorus of tButyl-phenyl-phosphinic Acid (—)-Menthyl Ester by Means of 1H NMR Spectroscopy

1977 ◽  
Vol 32 (5) ◽  
pp. 589-593 ◽  
Author(s):  
Reiner Luckenbach ◽  
Hans-H. Bechtolsheimer
Keyword(s):  
Nmr Spectroscopy ◽  
1H Nmr ◽  
Absolute Configuration ◽  
1H Nmr Spectroscopy ◽  
Nmr Spectra ◽  
Phosphinic Acid ◽  
H Nmr ◽  
The Absolute ◽  
Diastereomeric Purity

The preparation and separation into diastereomers of tbutyl-phenyl-phosphinic acid (—)-menthyl ester (1a) is reported. The diastereomeric purity as well as the absolute configuration at phosphorus of 1 a can be deduced from the detailed analysis of the 1H NMR spectra of samples of 1a differing in their diastereomer ratios.

scholarly journals Determination of Absolute Stereochemistry of Natural Alicyclic Glycosides by 1H NMR Spectroscopy without Application of Chiral Reagents – An Indication

2011 ◽  
Vol 6 (5) ◽  
pp. 1934578X1100600 ◽  
Author(s):  
Tatyana N. Makarieva ◽  
Larisa K. Shubina ◽  
Alla G. Guzii ◽  
Natalya V. Ivanchina ◽  
Vladimir A. Denisenko ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
1H Nmr ◽  
Absolute Configuration ◽  
1H Nmr Spectroscopy ◽  
Nmr Spectra ◽  
H Nmr ◽  
Steroid Glycosides ◽  
The Absolute ◽  
Absolute Stereochemistry

A study has been made of the 1H NMR spectra of peracetylated β-glucopyranosides and α-arabinopyranosides obtained by reaction of D- and L-glucoses, and L- and D-arabinoses with either ( R)- or ( S)-2-octanols. The obtained and literature data show that 1H NMR spectra may be used to determine the absolute configuration of the aglycone moieties of some alicyclic glycosides without the need to synthesize derivatives with chiral reagents, as long as the absolute configuration of their monosaccharide moiety is known or vice versa. Spectra of marine steroid glycosides and their acetates containing glycosylated side chains as alicyclic fragments were also examined. It was shown that analysis of 1H NMR spectra for the determination of the absolute configuration is more applicable in the cases when glycosides have the same substitution in the D-ring of the aglycone moiety.

Structure determination of diacholestanes by means of 13C-NMR and 1H-NMR spectroscopy

Tetrahedron ◽  
1981 ◽  
Vol 37 (24) ◽  
pp. 4331-4335 ◽  
Author(s):  
Daniel M. Tal ◽  
Hugo E. Gottlieb ◽  
Caroline Ben-Ari ◽  
Yehuda Mazur
Keyword(s):  
Nmr Spectroscopy ◽  
1H Nmr ◽  
13C Nmr ◽  
Structure Determination ◽  
1H Nmr Spectroscopy
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