High-pressure synthesis and crystal structure of α-Y2B4O9
2017 ◽
Vol 72
(12)
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pp. 977-982
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Keyword(s):
X Ray
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Abstractα-Y2B4O9 was synthesized in a high-pressure/high-temperature experiment at 12.3 GPa/1020°C. The crystal structure has been determined via single-crystal X-ray diffraction. α-Y2B4O9 is isotypic to the lanthanide borates α-Ln2B4O9 (Ln=Sm–Ho) and crystallizes in the monoclinic space group C2/c (no. 15) with the following lattice parameters: a=25.084(2), b=4.3913(2), c=24.726(2) Å, and β=99.97(1)°. The compound was further characterized via X-ray powder diffraction as well as IR and Raman spectroscopy.
2017 ◽
Vol 72
(1)
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pp. 69-76
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2008 ◽
Vol 63
(6)
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pp. 713-717
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2015 ◽
Vol 70
(3)
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pp. 183-190
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2010 ◽
Vol 65
(10)
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pp. 1206-1212
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2008 ◽
Vol 63
(6)
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pp. 707-712
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2007 ◽
Vol 62
(6)
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pp. 759-764
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