scholarly journals A multicommuted flow analysis method for the photometric determination of amoxicillin in pharmaceutical formulations using a diazo coupling reaction

2011 ◽  
Vol 22 (2) ◽  
pp. 279-285 ◽  
Author(s):  
Sueny K. B Freitas ◽  
Valdinete Lins da Silva ◽  
Alberto N Araújo ◽  
Maria Conceição B. S. M Montenegro ◽  
Boaventura F Reis ◽  
...  
Keyword(s):  
Flow Analysis ◽  
Coupling Reaction ◽  
Pharmaceutical Formulations ◽  
Photometric Determination ◽  
Analysis Method ◽  
Diazo Coupling ◽  
Diazo Coupling Reaction

scholarly journals Diazo coupling reaction for the determination of biliverdin.

1991 ◽  
Vol 40 (8) ◽  
pp. 377-381
Author(s):  
Yuji SUZUKI ◽  
Yoshikatsu SAKAGISHI
Keyword(s):  
Coupling Reaction ◽  
Diazo Coupling ◽  
Diazo Coupling Reaction

Analytic Methods for Bilirubin in Blood Plasma

1961 ◽  
Vol 7 (6) ◽  
pp. 603-625 ◽  
Author(s):  
Derek Watson
Keyword(s):  
Blood Plasma ◽  
Critical Evaluation ◽  
Coupling Reaction ◽  
Spectrophotometric Methods ◽  
Analytic Methods ◽  
Diazo Coupling ◽  
Diazo Coupling Reaction ◽  
In Blood Plasma

Abstract A critical evaluation of existing colorimetric and spectrophotometric methods for the determination of bilirubin in blood plasma is presented. The stoichiometric equivalences of the reagents used in the diazo coupling reaction are re-evaluated. The elimination of turbidity is discussed, as well as methods using diazo-coupling promoters. Recommendations are made concerning the preservation of specimens to prevent oxidation and procedures that give maximal specificity for the type of bilirubin pigment being assayed.

Green methods for the determination of nitrite in water samples based on a novel diazo coupling reaction

2017 ◽  
Vol 6 (2) ◽  
Author(s):  
Safwan M. Fraihat
Keyword(s):  
Water Samples ◽  
Acidic Medium ◽  
Coupling Reaction ◽  
Spectrophotometric Methods ◽  
New Methods ◽  
Diazo Coupling ◽  
Colored Product ◽  
Diazo Coupling Reaction

AbstractGreen, sensitive and selective spectrophotometric methods were developed for the determination of nitrite in water samples. The methods (A, B and C) are based on the reduction of 5-nitroimidazoles; metronidazole (MTL), secnidazole (SCL) and tinidazole (TNL), respectively, followed by diazotization using nitrite in acidic medium, then coupling with pyrogallol (PG). The amount of nitrite was determined by measuring the absorbance of the colored product at 385 nm. The new methods were linear in the ranges of 2.5–30 μgml

scholarly journals New Diazo Coupling Reactions for Visible Spectrophotometric Determination of Alfuzosin in Pharmaceutical Preparations

2007 ◽  
Vol 4 (4) ◽  
pp. 496-501 ◽  
Author(s):  
M. Vamsi Krishna ◽  
D. Gowri Sankar
Keyword(s):  
Pharmaceutical Preparations ◽  
Pharmaceutical Formulations ◽  
Molar Absorptivity ◽  
Basic Medium ◽  
Coupling Reactions ◽  
Acetyl Acetone ◽  
Diazo Coupling ◽  
Optimum Reaction ◽  
Diazonium Ion

Simple, rapid and sensitive spectrophotometric procedures were developed for the analysis of Alfuzosin hydrochloride (AFZ) in pure form as well as in pharmaceutical formulations. The methods are based on the reaction of AFZ with nitrite in acid medium to form diazonium ion, which is coupled with ethoxyethylenemaleic ester (Method A) or ethylcyanoacetate (Method B) or acetyl acetone (method C) in basic medium to form azo dyes, showing absorption maxima at 440, 465 and 490 nm respectively. Beer’s law is obeyed in the concentration of 4-20 μg/mL of AFZ for methods A, B and 3-15 μg/mL of AFZ for method C. The molar absorptivity and sandell’s sensitivity of AFZ- ethoxyethylenemaleic ester, AFZ- ethylcyanoacetate and AFZ-acetyl acetone are1.90 × 104, 0.022; 1.93 × 104, 0.021 and 2.67 × 104L mole-1cm-1, 0.015 μg cm-2respectively. The optimum reaction conditions and other analytical parameters were evaluated. The methods were successfully applied to the determination of AFZ in pharmaceutical formulations.

Synthesis of Azo Polyurethane-Urea and Investigation of its Thermo-Optic Properties

2016 ◽  
Vol 230 (2) ◽  
Author(s):  
Caihong Chen ◽  
Zhening Yang ◽  
Fengxian Qiu ◽  
Tianlin Cao ◽  
Guorong Cao ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Physical And Mechanical Properties ◽  
Isophorone Diisocyanate ◽  
Visible Spectroscopy ◽  
Diazo Coupling ◽  
Uv Visible ◽  
Diazo Coupling Reaction ◽  
The Fourier Transform ◽  
Azo Chromophore ◽  
Azo Polyurethane

AbstractAn azo chromophore molecular S(-)-1,2-bis(4-azophenyl-4-nitro)-ethylenediamine (OABANEDA) was synthesized with 4-nitroaniline and S(-)-1,2-diphenyl ethylenediamine by diazo-coupling reaction. The azo polyurethane-urea (OAAPUU) was obtained from OABANEDA, polyether diol (NJ-210) and isophorone diisocyanate (IPDI). The structure of OAAPUU was characterized by the Fourier transform infrared and UV-visible spectroscopy. The physical and mechanical properties of OAAPUU were investigated. The refractive index (

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