scholarly journals Interferences of Major Elements in the Determination of Rare Earth Elements by Inductively Coupled Plasma Atomic Emission Spectroscopy.

1992 ◽  
Vol 8 (2) ◽  
pp. 189-193 ◽  
Author(s):  
Ambrogio MAZZUCOTELLI ◽  
Fabio DE PAZ ◽  
Emanuele MAGI ◽  
Roberto FRACHE
1983 ◽  
Vol 37 (3) ◽  
pp. 261-263 ◽  
Author(s):  
Himansu S. Mahanti ◽  
Ramon M. Barnes

Inductively coupled plasma-atomic emission spectroscopy is evaluated for the determination of 14 rare earth elements in aluminum. Spectral line interference, limit of detection, and background equivalent concentration values are evaluated, and quantitative recovery is obtained from aluminum samples spiked with rare earth elements. The procedure is simple and suitable for routine process control analysis.


1983 ◽  
Vol 37 (4) ◽  
pp. 389-395 ◽  
Author(s):  
Ramon M. Barnes ◽  
Lancelot Fernando ◽  
Lu Shang Jing ◽  
Himansu S. Mahanti

Inductively coupled plasma-atomic emission spectroscopy (ICP-AES) is applied in the determination of 21 elements in primary, refined, and alloy aluminum. Rapid and reliable sample preparation procedures are developed. Spectral lines are selected after examination of experimental wavelength scans at each analyte wavelength. The limits of detection, background equivalent concentration, and analytical figures of merit are determined. For high silicon-containing aluminum, HF solutions were analyzed by employing an inert nebulizer utilizing polytetrafluoroethylene (PTFE) capillary tubes, a PTFE spray chamber, and an ICP torch with a graphite injector tube.


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