scholarly journals Dispersive Liquid–Liquid Microextraction of Cd, Hg and Pb from Medicines Prior to ICP Oes Determination According to the United States Pharmacopeia

2021 ◽  
Author(s):  
Fernanda Pinheiro ◽  
Miguel Ángel Aguirre ◽  
Joaquim Araújo Nóbrega ◽  
Antonio Canals

2021 ◽  
Author(s):  
Fernanda Pinheiro ◽  
Miguel Ángel Aguirre Pastor ◽  
Joaquim A. Nobrega ◽  
Antonio Canals

A simple, sensitive and matrix effect free analytical method for simultaneous determination of Cd, Hg and Pb in drug samples (i.e., commercial dosage tablets) by inductively coupled plasma optical emission...



1985 ◽  
Vol 53 (01) ◽  
pp. 116-117 ◽  
Author(s):  
R E Merton ◽  
A D Curtis ◽  
D P Thomas

SummaryHeparin samples from five manufacturers were assayed by the revised British Pharmacopoeia (BP) heparin assay and the results compared with those obtained using the activated partial thromboplastin time (APTT) assay. The United States Pharmacopeia (USP) reference heparin preparation and the 4th International Standard (IS) for heparin were also assayed by the two methods relative to the 3rd IS. The results obtained by the revised BP assay were in close agreement with those obtained by the APTT assay for all the heparins that were tested. The assays revealed that there is at least a 10% discrepancy between the International Unit for heparin and the USP unit.



JAMA ◽  
1913 ◽  
Vol 61 (14) ◽  
pp. 1289
Author(s):  
OLIVER T. OSBORNE


JAMA ◽  
1970 ◽  
Vol 213 (4) ◽  
pp. 576-579
Author(s):  
W. M. Heller


1975 ◽  
Vol 32 (8) ◽  
pp. 858-860
Author(s):  
Diane G. Thilman


1994 ◽  
Vol 77 (3) ◽  
pp. 756-757 ◽  
Author(s):  
Simon Chernomorsky

Abstract The reliability of the currently used quantitative assay for commercially available chlorophyllin copper complex is discussed. It was shown that optical measurements at 405 nm can overestimate the purity of the preparation by 16.4–49.5%. This conclusion is from comparative studies using spectrophotometry at 405 nm and elemental analysis (copper content) of chlorophyllin copper complex. Spectrophotometry at 630 nm resulted in closer agreement with data calculated from elemental analysis. These observations have to be taken into consideration by those involved in the manufacture and distribution of chlorophyllin copper complex as well as in the development of the United States Pharmacopeia compendial monograph for this preparation.



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