Rheological characterization of microfibrillated cellulose suspension using optical coherence tomography

TAPPI Journal ◽  
2015 ◽  
Vol 14 (5) ◽  
pp. 291-302 ◽  
Author(s):  
SANNA HAAVISTO ◽  
JUHA SALMELA ◽  
ARI JÄSBERG ◽  
TAPIO SAARINEN ◽  
ANNI KARPPINEN ◽  
...  

Fiber suspensions, such as microfibrillated cellulose, are a challenge for conventional rheometers to measure. This is because rheometers have small flow channel dimensions that can restrict flocculation. Often, questionable assumptions are also made about the fluid behavior in the gap. A pipe rheometer and ultrasound velocity profiling-pressure difference (UVP-PD) concept can be used, by which the real flow behavior is used for the rheological analysis of the bulk properties of the suspension. Unfortunately, the resolution of UVP is too low for studying near-wall phenomena, such as the lubrication layer, that are often very important for understanding the rheology and to upscale the results to industrial flows. To address this problem, we have widened the UVP-PD concept with optical coherence tomography measurements. This enables us to measure the bulk and wall-layer behavior simultaneously. Our results demonstrate the benefits of having direct, detailed measurement of the velocity profile inside the rheometer.

Cellulose ◽  
2014 ◽  
Vol 21 (3) ◽  
pp. 1261-1275 ◽  
Author(s):  
Tapio Saarinen ◽  
Sanna Haavisto ◽  
Anni Sorvari ◽  
Juha Salmela ◽  
Jukka Seppälä

Cellulose ◽  
2017 ◽  
Vol 24 (11) ◽  
pp. 4715-4728 ◽  
Author(s):  
Janne Lauri ◽  
Antti Koponen ◽  
Sanna Haavisto ◽  
Jakub Czajkowski ◽  
Tapio Fabritius

Cellulose ◽  
2021 ◽  
Vol 28 (6) ◽  
pp. 3373-3387
Author(s):  
Janne Lauri ◽  
Sanna Haavisto ◽  
Juha Salmela ◽  
Arttu Miettinen ◽  
Tapio Fabritius ◽  
...  

AbstractIn this study, cellulose microfibril (CMF) suspensions were imaged during pipe flow at consistencies of 0.4%, 1.0%, and 1.6% with optical coherence tomography (OCT) to obtain images of the structure and the local velocity of the suspension. The viscosities obtained by combining pressure loss measurement with the OCT velocity data showed typical shear thinning behavior and were in excellent agreement with viscosities obtained with ultrasound velocity profiling. The structural OCT images were used to calculate the radial and the axial floc sizes of the suspension. A fit of power law to the geometrical floc size–shear stress data gave the same power law index for all consistencies, suggesting that floc rupture dynamics is independent of consistency. The dependence of viscosity and floc size on shear stress was similar, indicating that the shear thinning behavior of CMF suspensions is closely related to the rupture dynamics of flocs. The results also showed that an apparent attenuation coefficient of the OCT signal can be used to determine the consistency of CMF suspensions.


Author(s):  
Julia N.S. d'Hooghe ◽  
Daniel M. de Bruin ◽  
Joris J.T.H. Roelofs ◽  
Jouke T. Annema ◽  
Peter I. Bonta

2018 ◽  
Vol 8 (5) ◽  
pp. 755 ◽  
Author(s):  
Antti Koponen ◽  
Janne Lauri ◽  
Sanna Haavisto ◽  
Tapio Fabritius

2007 ◽  
Vol 177 (4S) ◽  
pp. 358-359 ◽  
Author(s):  
Christopher S. Lee ◽  
Alek Mishail ◽  
Jason M. Kim ◽  
Alexander Kirshenbaum ◽  
Howard L. Adler ◽  
...  

2006 ◽  
Vol 175 (4S) ◽  
pp. 395-395
Author(s):  
Nancy J. Tresser ◽  
Elena V. Zagaynova ◽  
Olga S. Streltsova ◽  
Natalia D. Gladkova ◽  
Vladislav A. Kamensky ◽  
...  

2004 ◽  
Vol 171 (4S) ◽  
pp. 68-68 ◽  
Author(s):  
Markus D. Sachs ◽  
Dmitry Daniltchenko ◽  
Eva Lankenau ◽  
Frank Koenig ◽  
Gerion Huettmann ◽  
...  

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