Simultaneous determination of 15 industrial synthetic dyes in condiment by solid phase extraction-high performance liquid chromatography

2011 ◽  
Vol 29 (2) ◽  
pp. 162-167 ◽  
Author(s):  
Min LIU ◽  
Xiaolin LI ◽  
Wei BIE ◽  
Minglin WANG ◽  
Qian FENG
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Solid Phase Extraction ◽  
Simultaneous Determination ◽  
High Performance ◽  
Solid Phase ◽  
Synthetic Dyes ◽  
Phase Extraction

scholarly journals Simultaneous Determination of Nitroimidazole Residues in Honey Samples by High-Performance Liquid Chromatography with Ultraviolet Detection

2007 ◽  
Vol 90 (3) ◽  
pp. 872-878 ◽  
Author(s):  
Jinhui Zhou ◽  
Jianzhong Shen ◽  
Xiaofeng Xue ◽  
Jing Zhao ◽  
Yi Li ◽  
...  
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Solid Phase Extraction ◽  
Simultaneous Determination ◽  
High Performance ◽  
Solid Phase ◽  
Phase Extraction ◽  
Ultraviolet Detection ◽  
Ultraviolet Detector

Abstract A rapid and sensitive high-performance liquid chromatography (LC) method was developed for the simultaneous determination of metronidazole (MNZ), dimetridazole (DMZ), ronidazole (RNZ), tinidazole (TNZ), and 2-hydroxymethyl-1-methyl-5-nitroimidazole (HMMNI) in honey. After extraction with ethyl acetate and evaporation, the residue containing the nitroimidazoles was dissolved in ethyl acetatehexane and subjected to solid-phase extraction cleanup by amine extraction columns. The effluent was evaporated to dryness, and residues were dissolved and determined by LC with an ultraviolet detector set at 315 nm. The limits of detection were 1.02.0 ng/g for MNZ, DMZ, RNZ, TNZ, and HMMNI in honey. Average recoveries ranged from 71.5101.4% in honey fortified at 10, 20, 50, and 100 ng/g. The method was validated for the analysis of real honey samples.

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