Rapid grain orientation imaging using spatially resolved acoustic spectroscopy

Author(s):  
Steve D. Sharples ◽  
Matt Clark ◽  
Mike G. Somekh ◽  
Elizabeth E. Sackett ◽  
Lionel Germain ◽  
...  
2017 ◽  
Vol 140 ◽  
pp. 67-70 ◽  
Author(s):  
Rikesh Patel ◽  
Wenqi Li ◽  
Richard J. Smith ◽  
Steve D. Sharples ◽  
Matt Clark

2012 ◽  
Vol 353 ◽  
pp. 012003 ◽  
Author(s):  
R Smith ◽  
S Sharples ◽  
W Li ◽  
M Clark ◽  
M Somekh

2014 ◽  
Vol 25 (5) ◽  
pp. 055902 ◽  
Author(s):  
Richard J Smith ◽  
Wenqi Li ◽  
Jethro Coulson ◽  
Matt Clark ◽  
Michael G Somekh ◽  
...  

2007 ◽  
Vol 539-543 ◽  
pp. 493-498 ◽  
Author(s):  
Ivan Saxl ◽  
Vàclav Sklenička ◽  
L. Ilucová ◽  
Milan Svoboda ◽  
Petr Král

Considerable structural inhomogeneity and anisotropy were found even after eight ECAP passes in high purity aluminium and the creep loading of ECAP material at 473K, 15MPa resulted in scattered fracture times ~ 20-60 hours. The structure revealed by orientation imaging microscopy with different disclination bounds was analysed by stereological methods. The effect of inhomogeneity and grain orientation on the creep fracture time was assessed.


2014 ◽  
Vol 520 ◽  
pp. 012017 ◽  
Author(s):  
Wenqi Li ◽  
Jethro Coulson ◽  
John W Aveson ◽  
Richard J Smith ◽  
Matt Clark ◽  
...  

2006 ◽  
Vol 910 ◽  
Author(s):  
Etienne Pihan ◽  
Abdelilah Slaoui ◽  
Claude Maurice

AbstractWe investigated the structural quality of polysilicon films fabricated by the aluminium induced crystallization (AIC) of amorphous silicon on alumina substrates. We analyzed the overall crystallographic quality of the poly-Si films in terms of grain size distribution and grain orientation versus crystallization temperature. For these studies, we used extensively the orientation imaging micrograph (OIM) technique, a very powerful tool that allows elucidating the inner-grain structure, the grain boundaries, the grain orientation. From our analysis, we may conclude that the polysilicon films formed by AIC on alumina substrates have the following features: (i) for all investigated temperatures, most of the silicon grains have a deviation angle from (100) crystallographic orientation between 5 and 25°; (ii) increasing the annealing temperature tends to decrease the (100) preferred orientation; (iii) the angular boundary distribution revealed that the main defects are those that have been observed inside isolated dentrites, namely low angle boundaries (<2°) and coincident site lattice boundaries such as Σ3, Σ9 and Σ27.


1995 ◽  
Vol 403 ◽  
Author(s):  
P.-C. Wang ◽  
G. S. Cargill ◽  
I. C. Noyan ◽  
E. G. Liniger

AbstractWe describe spatially resolved grain orientation mapping of polycrystalline films using a synchrotron-based x-ray microdiffraction system. The system consists of a tapered glass capillary as a white x-ray concentrator, an energy-dispersive solid state detector and an x-y-z sample stage. Two mapping modes are discussed: reciprocal-space mapping and real-space mapping. Information about the orientations of grains within the irradiated volume is determined by reciprocal-space mapping. The locations of grains having a specified orientation are determined by real-space mapping. Examples are shown for blanket films of AI(4 wt.% Cu) 4μm-thick and 0.5μm thick. Results are also shown for 10μm-wide and μm-wide pure lines. X-ray beams of 10inm diameter were used for these measurements. Spatially resolved thermal strain measurements were made for a single 10μm-wide, 200μm-long passivated Al line, and they were found to be consistent with calculations based on equi-biaxial thermal stress within the line.


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