Neutron Diffraction Study of a CuAlBe Shape Memory Alloy

2011 ◽  
Vol 172-174 ◽  
pp. 178-183 ◽  
Author(s):  
Matthieu Dubois ◽  
Marie Hélène Mathon ◽  
Vincent Klosek ◽  
Gilles Andre ◽  
Alain Lodini

This work presents the texture evolution of the austenitic phase of a copper based shape memory alloy by neutron diffraction. The Cu-11%Al-0.62%Be (in mass %) alloy was subjected to cold and hot rolling processes. The texture of the rolled samples at reduction rates of 5%, 10% and 15% respectively were compared to those of the raw material. A <001> partial fiber is observed for the raw material and cold rolled samples whereas the texture of the hot rolled sample is mainly characterized by a <111> fiber. The influence of these mechanical treatments on the transition temperatures and the hysteresis evolution was also analysed by following the integrated intensity of the {220} reflection of the austenitic phase. A shift towards low temperatures of martensitic transition temperatures is observed with the increasing of the rolling rate.

2011 ◽  
Vol 409 ◽  
pp. 569-574
Author(s):  
Matthieu Dubois ◽  
Marie Hélène Mathon ◽  
Vincent Klosek ◽  
Gilles Andre ◽  
Alain Lodini

This work was devoted to the study of a copper based shape memory alloy using the neutron diffraction method. We present the crystallographic texture evolution of the austenite phase of the Cu-11%Al-0.62%Be (wt. %) alloy which was subjected to cold and hot rolling processes. The texture of the cold rolled samples at reduction rates of 5%, 10% and 15% respectively was measured and compared to the raw material. A <001> partial fiber is observed for the raw material and for cold rolled samples whereas the texture of the hot rolled sample is mainly characterized by a <111> fiber. On the second part, we have studied the influence of the rolling treatment on the transition temperatures by following the integrated intensity of the {220} austenite reflection. The increase of the rolling rate seems to shift the characteristic temperatures towards low temperatures.


2006 ◽  
Vol 421 (1-2) ◽  
pp. 15-21 ◽  
Author(s):  
D.W. Brown ◽  
M.A.M. Bourke ◽  
R.D. Field ◽  
W.L. Hults ◽  
D.F. Teter ◽  
...  

2014 ◽  
Vol 216 ◽  
pp. 194-199
Author(s):  
Matthieu Dubois ◽  
Don Brown ◽  
Bjørn Clausen ◽  
Ahmed Addad ◽  
Alain Lodini

The aim of this work is to understand the evolutions of the β1metastable austenite phase of a CuAlBe Shape Memory Alloy at macroscopic and microscopic scales under mechanical solicitation by neutron diffraction. The tensile specimen, taken in the raw material is subjected to superelastic cycles at room temperature on SMARTS diffractometer. Before loading, the mater ial is fully austenitic. During loading, after elastic deformation of austenite, phase transformation starts, martensite variants appear. The material follows a law of pseudo elastic behavior. At the end of the first mechanical cycle after unloading, the macroscopic curve does not fully return into its original point. A macroscopic deformation is observed. The evolution of first order microdeformations during mechanical cycles shows a large deformation of {400} plane family. This deformation is linked to the presence of <001> partial fibber characterizing the crystallographic texture of the material after elaboration. The FWHM of the (400) diffraction peak is also largely increased during loading. This increase is the signature of the generation of stacking faults during the transformation of β1metastable austenite into β1martensite.


2002 ◽  
Vol 66 (5) ◽  
Author(s):  
Jordi Marcos ◽  
Antoni Planes ◽  
Lluís Mañosa ◽  
Amílcar Labarta ◽  
Bart Jan Hattink

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