solvothermal technique
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2022 ◽  
Author(s):  
Yuzhen Zhao ◽  
Min Zhu ◽  
Hailing Shang ◽  
Xiang Cheng ◽  
Daniele Ramella ◽  
...  

A solvothermal technique was used to prepare UiO-67, a metal-organic framework based on Zirconium; immobilized Fe3+ active sites were added using a facile post-synthetic modification method. The as-synthesized catalyst UiO-67@Fe...


AIP Advances ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 025003
Author(s):  
R. D. Ralandinliu Kahmei ◽  
Sarath Arackal ◽  
S. A. Shivashankar ◽  
Navakanta Bhat ◽  
Ranajit Sai

RSC Advances ◽  
2020 ◽  
Vol 10 (16) ◽  
pp. 9693-9703 ◽  
Author(s):  
W. S. Abo El-Yazeed ◽  
Y. G. Abou El-Reash ◽  
L. A. Elatwy ◽  
Awad I. Ahmed

This work reported the preparation of Mg-MOF, Fe-MOF and Fe–Mg MOF by a solvothermal technique and their characterization with FT-IR, XRD, SEM, EDS, TEM and SBET analyses.


Author(s):  
Yogeshwar R. Suryawanshi ◽  
Mousumi Chakraborty ◽  
Smita Jauhari ◽  
Sulekha Mukhopadhyay ◽  
Kalsanka. T. Shenoy

Abstract Ruthenium-palladium (Ru-Pd) and ruthenium-nickel (Ru-Ni) bimetallic nanoalloy particles with various metal compositions were synthesized by microwave irradiated (MWI) solvothermal technique using PVP (poly-N-vinyl-2-pyrrolidone) as capping agent and ethylene glycol as a solvent as well as reducing agent. Synthesized bimetallic nanoalloy particles were subsequently impregenated onto γ-Al2O3 support to obtain supported nanoalloy catalysts. Agglomeration of nanoalloyparticles were restricted by using excess solvent during synthesis, then distilled and recovered after completion of reaction. Hydrogenation of Dibenzo-18-crown-6 ether (DB18C6) was carried out at 9 MPa, 120°C and 3.5 h using synthesized bimetallic nanoalloy catalysts. It was observed that bimetallic nanolloycatalyst synthesized by MWI using Ru:Pd 3:1 % (w/w), exhibited higher catalytic activity and resulted 98.9 % conversion of DB18C6 with 100 % selectivity towards cis-syn-cis dicyclohexano-18-crown-6 ether (CSC DCH18C6).


2019 ◽  
Author(s):  
Zainab Sabeeh Sadeq ◽  
Saif M. Alshrefi ◽  
Wasan R. Saleh ◽  
Dunia K. Mahdi

RSC Advances ◽  
2019 ◽  
Vol 9 (71) ◽  
pp. 41490-41501 ◽  
Author(s):  
Zakariyya Uba Zango ◽  
Khairulazhar Jumbri ◽  
Nonni Soraya Sambudi ◽  
Noor Hana Hanif Abu Bakar ◽  
Nor Ain Fathihah Abdullah ◽  
...  

Three adsorbents based on the metal–organic frameworks (MOFs), viz.; MIL-88(Fe), NH2-MIL-88(Fe), and mixed-MIL-88(Fe) were synthesized using a microwave-assisted solvothermal technique.


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