A method for the identification of the double-bond position of isomeric linear tetradecenols and related compounds based on mass spectra of dimethyl disulfide derivatives

2001 ◽  
Vol 16 (1) ◽  
pp. 11-14 ◽  
Author(s):  
Gu Yuan ◽  
Jichao Yan

1983 ◽  
Vol 55 (6) ◽  
pp. 818-822 ◽  
Author(s):  
Hans Rudolf. Buser ◽  
Heinrich. Arn ◽  
Patrick. Guerin ◽  
Stefan. Rauscher


1985 ◽  
Vol 57 (8) ◽  
pp. 1621-1625 ◽  
Author(s):  
Boel S. Lanne ◽  
Monica. Appelgren ◽  
Gunnar. Bergstroem ◽  
Christer. Loefstedt


1987 ◽  
Vol 59 (5) ◽  
pp. 694-699 ◽  
Author(s):  
Marco. Vincent ◽  
Gianfranco. Guglielmetti ◽  
Giorgio. Cassani ◽  
Cristina. Tonini


1971 ◽  
Vol 26 (7) ◽  
pp. 679-683 ◽  
Author(s):  
Herbert W. Roesky ◽  
Enno Janssen

P3N3F5NCO was prepared by reaction of P3N3F5NSO with (COCl) 2. Substituted amides were obtained from the reaction of P3N3F5NSO with carbonic acids e. g. P3N3F5NHCOCH3, P3N3F5NHCOC2H5, and P3N3F5NHCOC3H7. If these substances were treated with PCl5 the following compounds P3N3F5N = CClCH3, P3N3F5N = CClCH5, and P3N3F5TN = CClC3H7 were formed. They reacted with nucleophiles to give P3N3F5N = CNH2CH3, P3N3F5N = TN (CH3) 2C2H5, and P3N3F5N = CN (CH3) 2CH7. The properties of these compounds are described. They were characterized by elemental analysis and IR-spectra. 19F-, 1H-NMR, and mass spectra are reported.



1971 ◽  
Vol 8 (2) ◽  
pp. 225-230 ◽  
Author(s):  
Charks W. Koch ◽  
I. Hodge Markgraf


1968 ◽  
Vol 89 (6) ◽  
pp. 594-596 ◽  
Author(s):  
Yoshimori OMOTE ◽  
Hiroko YASUDA ◽  
Yoshimori FUJINUMA ◽  
Noboru SUGIYAMA




1973 ◽  
Vol 51 (9) ◽  
pp. 1313-1321 ◽  
Author(s):  
Morris J. Robins ◽  
James R. McCarthy Jr. ◽  
Roger A. Jones ◽  
Rudolf Mengel

Reaction of tubercidin (4-amino-7-β-D-ribofuranosylpyrrolo[2,3-d]pyrimidine) (1) with α-acetoxyisobutyryl chloride in the presence of excess sodium iodide in acetonitrile gave an acylated iodo intermediate (2) which was converted into 3′-deoxytubercidin (4) by hydrogenolysis and subsequent saponification.Analogous treatment of formycin (7-amino-3-β-D-ribofuranosylpyrazolo[4,3-d]pyrimidine) (5) gave 3′-deoxyformycin (6) and 2′-deoxyformycin (7) in an approximate ratio of 3:2. These purified nucleosides, 6 and 7 were individually deaminated enzymatically to give 3′-deoxyformycin B (8) and 2′-deoxyformycin B(9).Biological rationale, n.m.r., and mass spectra of these antibiotic-derived deoxynucleosides are discussed.



1973 ◽  
Vol 7 (6) ◽  
pp. 719-735 ◽  
Author(s):  
G. Pattenden ◽  
L. Crombie ◽  
P. Hemesley


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