Multiple-π-Pulse Sequences in Biological Solid-State NMR. Enhancement of Sensitivity by Permutation of the Phases

1996 ◽  
Vol 111 (3) ◽  
pp. 296-299 ◽  
Author(s):  
Yan Li ◽  
Jeremy N.S. Evans
Nanomaterials ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 1494
Author(s):  
Mustapha El Hariri El Nokab ◽  
Khaled O. Sebakhy

Solid-state NMR has proven to be a versatile technique for studying the chemical structure, 3D structure and dynamics of all sorts of chemical compounds. In nanotechnology and particularly in thin films, the study of chemical modification, molecular packing, end chain motion, distance determination and solvent-matrix interactions is essential for controlling the final product properties and applications. Despite its atomic-level research capabilities and recent technical advancements, solid-state NMR is still lacking behind other spectroscopic techniques in the field of thin films due to the underestimation of NMR capabilities, availability, great variety of nuclei and pulse sequences, lack of sensitivity for quadrupole nuclei and time-consuming experiments. This article will comprehensively and critically review the work done by solid-state NMR on different types of thin films and the most advanced NMR strategies, which are beyond conventional, and the hardware design used to overcome the technical issues in thin-film research.


Author(s):  
Andreas Brinkmann ◽  
Marina Carravetta ◽  
Xin Zhao ◽  
Mattias Edén ◽  
Jörn Schmedt auf der Günne ◽  
...  

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.


2013 ◽  
Vol 228 ◽  
pp. 66-75 ◽  
Author(s):  
Matthias Bechmann ◽  
John Clark ◽  
Angelika Sebald

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