Challenges in numerical simulations of solid-state NMR experiments: Spin exchange pulse sequences

2010 ◽  
Vol 38 (4) ◽  
pp. 77-83 ◽  
Author(s):  
Thomas Vosegaard
Keyword(s):  
Solid State ◽  
Numerical Simulations ◽  
Solid State Nmr ◽  
Spin Exchange ◽  
Pulse Sequences

scholarly journals Solid State NMR Spectroscopy a Valuable Technique for Structural Insights of Advanced Thin Film Materials: A Review

Nanomaterials ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 1494
Author(s):  
Mustapha El Hariri El Nokab ◽  
Khaled O. Sebakhy
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Solid State ◽  
Solid State Nmr ◽  
Pulse Sequences ◽  
3D Structure ◽  
Spectroscopic Techniques ◽  
Film Research ◽  
Versatile Technique ◽  
Work Done

Solid-state NMR has proven to be a versatile technique for studying the chemical structure, 3D structure and dynamics of all sorts of chemical compounds. In nanotechnology and particularly in thin films, the study of chemical modification, molecular packing, end chain motion, distance determination and solvent-matrix interactions is essential for controlling the final product properties and applications. Despite its atomic-level research capabilities and recent technical advancements, solid-state NMR is still lacking behind other spectroscopic techniques in the field of thin films due to the underestimation of NMR capabilities, availability, great variety of nuclei and pulse sequences, lack of sensitivity for quadrupole nuclei and time-consuming experiments. This article will comprehensively and critically review the work done by solid-state NMR on different types of thin films and the most advanced NMR strategies, which are beyond conventional, and the hardware design used to overcome the technical issues in thin-film research.

scholarly journals Using symmetry to design pulse sequences in solid-state NMR

2001 ◽  
pp. 3-14
Author(s):  
Andreas Brinkmann ◽  
Marina Carravetta ◽  
Xin Zhao ◽  
Mattias Edén ◽  
Jörn Schmedt auf der Günne ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Pulse Sequences

Numerical Simulations in Solid-State NMR with Simpson

2010 ◽  
Author(s):  
Thomas Vosegaard ◽  
Zdeněk Tošner ◽  
Niels Chr. Nielsen
Keyword(s):  
Solid State ◽  
Numerical Simulations ◽  
Solid State Nmr

scholarly journals Rapid acquisition of wideline MAS solid-state NMR spectra with fast MAS, proton detection, and dipolar HMQC pulse sequences

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Pulse Sequences ◽  
Quadrupolar Nuclei ◽  
Proton Detection ◽  
Rapid Acquisition ◽  
Half Integer ◽  
Fast Mas

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.

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