Synthesis and Characterization of the New Ternary Nitride (Fe0.8W0.2)WN2

1997 ◽  
Vol 131 (2) ◽  
pp. 374-378 ◽  
Author(s):  
Joel D. Houmes ◽  
Sandhya Deo ◽  
Hans-Conrad zur Loye
Keyword(s):  
Synthesis And Characterization ◽  
Ternary Nitride

Synthesis and Characterization of the Ternary Nitride, Sr2TaN3.

ChemInform ◽  
2003 ◽  
Vol 34 (13) ◽  
Author(s):  
Amy Bowman ◽  
Duncan H. Gregory
Keyword(s):  
Synthesis And Characterization ◽  
Ternary Nitride

Synthesis and Characterization of a New Ternary Transition Metal Nitride, FeWN2, from the Transition Metal Oxide Precursor, FeWO4

1993 ◽  
Vol 327 ◽  
Author(s):  
David S. Bem ◽  
Joel D. Houmes ◽  
Hans-Conrad Zur Loye
Keyword(s):  
Transition Metal ◽  
Synthesis And Characterization ◽  
Rietveld Refinements ◽  
Metal Tungstate ◽  
Transition Metal Nitride ◽  
Oxide Precursor ◽  
Iron Coordination ◽  
Mössbauer Data ◽  
Ternary Nitride

AbstractThe ternary nitride, FeWN2, has been synthesized via ammonolysis of the transition metal tungstate, FeWO4. FeWN2 is hexagonal with a unit cell of a = 2.8724(1) Å and c =10.973(4) A. Rietveld refinements were performed in the space group P3–1C with Rwp=9.91%, and Rp=7.23%. The structure consist of alternating octahedrally coordinated iron-nitrogen layers and trigonal prismatically coordinated tungsten-nitrogen layers. Mössbauer data at 250K indicates an isomer shift δ=0.85 and shows no quadrupole splitting, which is consistent with the octahedral iron coordination in the proposed structure.

Synthesis and Characterization of the Three Dicyclopentapyrenes

1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula
Keyword(s):  
Synthesis And Characterization

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

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