Introduction to instrumental methods of analysis

Author(s):  
M. H. Gordon ◽  
R. Macrae
Author(s):  
Bibin K. B.

Background: Sneha Kalpana is one among the several highly established Kalpana of Ayurvedic system of medicine. Many types of Taila Kalpana are mentioned in Ayurvedic classics and used effectively in therapeutic practice. Tila Taila is the most commonly using Taila. However Narikelataila, Erandataila, Sarshapataila, etc, are also used in special conditions. It is interesting to note that certain preparations are available in the market based on both TilaTaila and Narikela Taila. This is an attempt to comparatively evaluate the formulation Dhutturadi Taila prepared in Tila Taila and Narikela Taila as the bases. Dhutturadi Taila mentioned in Sahasrayogam is taken for the present study. Objectives: To comparatively analyse Dhutturadi Taila samples with classical and advanced analytical techniques. Materials and Methods: Dhutturadi Taila was prepared using two media i.e. Narikela Taila and Tila Taila. Both Taila samples were comparatively analysed with suitable physicochemical parameters and advanced instrumental methods of analysis. Conclusion: As per the existing result it seems that more amount of marker components are extracted into Tila Taila medium when compared with Narikela Taila.


Química Nova ◽  
2020 ◽  
Author(s):  
Julia Postigo ◽  
Hellen Barbosa ◽  
Roberta Calefi ◽  
Jany Jesus ◽  
Priscila Cervini ◽  
...  

A PROPOSITION FOR TEACHING LABORATORY OF QUALITATIVE ANALYTICAL CHEMISTRY. Teaching laboratory of qualitative analytical chemistry is still a controversial issue in chemistry courses. However, important researchers and educators in chemistry recognized and highlighted the importance that the contents of this discipline represent in the formation of chemists, once it can provide handling and understanding of microscopic phenomena based on the observation of their macroscopic effects, once such reactions and phenomena are the basis of important instrumental methods of analysis. Thus, a proposal based on a bottom-up approach has been developed, starting with the observation of different reactions of cations in laboratory, followed by a search for the reaction responsible for each resulting phenomenon observed during the experimental step. Then these reactions are related with the separation procedures of each group of cations. Eventually the separation of these groups can also be performed depending on the time available. The proposal has been applied in teaching laboratory of qualitative analytical chemistry at Instituto de Química de São Carlos/USP since 2015, where the discipline is offered duirng 4 hours/week, and a positive feedback regarding the evolution of the methodology and its acceptance by students. Good results were also obtained concerning the appropriation of the contents by the students, using the proposal.


Author(s):  
V.V. Avtukhovich ◽  
◽  
M.P. Krasnovskikh ◽  
O. U. Kamenschikov ◽  
A. L. Gabov ◽  
...  

The use of a complex of chemical and instrumental methods of analysis opens up wide possibilities for studying the transformations of charge components that occur during the production of light ceramic bricks of PKK on Zakamennaya LLC. The applicability of modern thermal analysis methods is described and determined, and recommendations are given for solving technological problems of this ceramic production.


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