A Hard X-Ray Telescope/Concentrator Design Based on Graded Period Multilayer Coatings

Author(s):  
F. E. Christensen ◽  
K. D. Joensen ◽  
P. Gorenstein ◽  
W. C. Priedhorsky ◽  
N. J. Westergaard ◽  
...  
Keyword(s):  
Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1153
Author(s):  
Ivan Pavlenko ◽  
Jozef Zajac ◽  
Nadiia Kharchenko ◽  
Ján Duplák ◽  
Vitalii Ivanov ◽  
...  

This article deals with improving the wear resistance of multilayer coatings as a fundamental problem in metal surface treatment, strengthening elements of cutting tools, and ensuring the reliability of machine parts. It aims to evaluate the wear depth for multilayer coatings by the mass loss distribution in layers. The article’s primary purpose is to develop a mathematical method for assessing the value of wear for multilayer steel-based coatings. The study material is a multilayer coating applied to steel DIN C80W1. The research was performed using up-to-date laboratory equipment. Nitrogenchroming has been realized under overpressure in two successive stages: nitriding for 36 h at temperature 540 °C and chromizing during 4 h at temperature 1050 °C. The complex analysis included several options: X-ray phase analysis, local micro-X-ray spectral analysis, durometric analysis, and determination of wear resistance. These analyses showed that after nitrogenchroming, the three-layer protective coating from Cr23C6, Cr7C3, and Cr2N was formed on the steel surface. Spectral analysis indicated that the maximum amount of chromium 92.2% is in the first layer from Cr23C6. The maximum amount of carbon 8.9% characterizes the layer from Cr7C3. Nitrogen is concentrated mainly in the Cr2N layer, and its maximum amount is 9.4%. Additionally, it was determined that the minimum wear is typical for steel DIN C80W1 after nitrogenchroming. The weight loss of steel samples by 25 mg was obtained. This value differs by 3.6% from the results evaluated analytically using the developed mathematical model of wear of multilayer coatings after complex metallization of steel DIN C80W1. As a result, the impact of the loading mode on the wear intensity of steel was established. As the loading time increases, the friction coefficient of the coated samples decreases. Among the studied samples, plates from steel DIN C80W1 have the lowest friction coefficient after nitrogenchroming. Additionally, a linear dependence of the mass losses on the wearing time was obtained for carbide and nitride coatings. Finally, an increase in loading time leads to an increase in the wear intensity of steels after nitrogenchroming. The achieved scientific results are applicable in developing methods of chemical-thermal treatment, improving the wear resistance of multilayer coatings, and strengthening highly loaded machine parts and cutting tools.


1999 ◽  
Vol 28 (1) ◽  
pp. 1-13
Author(s):  
D. Bhattacharyya ◽  
N. C. Das ◽  
A. P. Roy ◽  
R. Chitra ◽  
S. Basu
Keyword(s):  

2019 ◽  
Vol 19 (1) ◽  
pp. 554-561 ◽  
Author(s):  
Catherine Burcklen ◽  
Regina Soufli ◽  
Jennifer Rebellato ◽  
Christopher Walton ◽  
Evgueni Meltchakov ◽  
...  
Keyword(s):  

1999 ◽  
Author(s):  
Adrian Ivan ◽  
Ricardo J. Bruni ◽  
Kyung Wha Byun ◽  
Finn E. Christensen ◽  
Paul Gorenstein ◽  
...  

Author(s):  
Mónica Fernández-Perea ◽  
Mike J. Pivovaroff ◽  
Regina Soufli ◽  
Jennifer Alameda ◽  
Paul Mirkarimi ◽  
...  

1998 ◽  
Vol 551 ◽  
Author(s):  
A. Ivan ◽  
R. Bruni ◽  
K. Byun ◽  
J. Everett ◽  
P. Gorenstein ◽  
...  

AbstractSeveral multilayer test coatings for hard X-ray telescopes were fabricated using DC magnetron sputtering. The process parameters were selected from a series of trials of single layer depositions. The samples were characterized using X-ray specular reflectivity scans, AFM, and cross-sectional TEM. Additional measurements (stylus profilometry, RBS, and Auger analysis) were used in the optimization of the deposition rate and of the thin film properties (density, composition, surface/interface microroughness). The X-ray reflectivity scans showed that the combinations of reflector and spacer materials tested so far (W/Si and W/C) are suited for graded d-spacing multilayer coatings that present a constant reflectivity bandpass up to 70 keV.


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