A new method of determination of the oil content in porous powder metallurgy parts

1987 ◽  
Vol 26 (8) ◽  
pp. 675-677
Author(s):  
V. D. Zozulya ◽  
V. G. Prikhod'ko
2017 ◽  
Vol 68 (4) ◽  
pp. 671-674
Author(s):  
Ana Maria Galan ◽  
Ioan Calinescu ◽  
Elena Radu ◽  
Elena Emilia Oprescu ◽  
Gabriel Vasilievici ◽  
...  

The purpose of this study was to develop a method for rapid quantitative and qualitative determination of the oil from microalgae lipid fraction obtained from Nannochloris sp biomass. The lipid fraction was first refluxed with 4% KOH in MeOH (60, 90, 120 min), followed by reaction with 20% BF3 in MeOH, using different times of reflux (90,120, 150 min) for each time of reflux with 4% KOH in MeOH. The FAME samples were analyzed by GC-MS analysis. 120 min reflux with 4% KOH in MeOH, 90 min with 20% BF3 in MeOH and a ratio lipid fraction: 4% KOH in MeOH: 20% BF3 in MeOH=1:20:27, were required to obtain the higher percent of oil in the microalgae lipid fraction. The relevance of the method developed was proved by TGA analysis and by transesterification of a sunflower oil sample in the same conditions.


2012 ◽  
Vol 48 (1-2) ◽  
pp. 15-21
Author(s):  
V. N. Skopinskii ◽  
N. A. Berkov ◽  
A. D. Emelyanova

2005 ◽  
pp. 39-73 ◽  
Author(s):  
Jürn W. P. Schmelzer ◽  
Vitali V. Slezov ◽  
Alexander S. Abyzov

1980 ◽  
Vol 85 ◽  
pp. 249-250
Author(s):  
E. S. Parsamian

A new method of determination of the ages of aggregates based on flare star observations is proposed. The method is specially useful in the case of young clusters and associations, for which the usual method involving their H-R diagrams encounters difficulties. The method can be used also for particular flare stars.


Sign in / Sign up

Export Citation Format

Share Document