Combination of neutron activation, atomic absorption spectroscopy and conventional methods in the elemental analysis of silicate rocks

1986 ◽  
Vol 97 (2) ◽  
pp. 265-270 ◽  
Author(s):  
M. A. Gouveia ◽  
J. Seabra e Barros ◽  
M. Jesus Tavares ◽  
M. Carmo Freitas
Keyword(s):  
Neutron Activation ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Elemental Analysis ◽  
Atomic Absorption Spectroscopy ◽  
Conventional Methods ◽  
Silicate Rocks

scholarly journals Research of the Content of Heavy Metals in the Atmospheric Precipitation of the Geygel, Dashkesan and Gedabek Districts of Azerbaijan

2021 ◽  
Vol 7 (6) ◽  
Author(s):  
Sh. Nuguyeva ◽  
E. Mammadov
Keyword(s):  
Heavy Metals ◽  
Neutron Activation ◽  
Atmospheric Deposition ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Atomic Absorption Spectroscopy ◽  
Epithermal Neutron ◽  
Atmospheric Precipitation ◽  
Nuclear Research ◽  
Atmospheric Air

The increasing content of heavy metals in soil and atmospheric air can lead to serious consequences in the final link of which a person is. To determine heavy metals in atmospheric deposition, the method of biomonitoring of mosses was used. Joint Institute for Nuclear Research scientists started the implementation of the mosses biomonitoring methodology in Azerbaijan 2015. In total, the concentration was determined for 44 elements. Determinations were performed using instrumental analysis of Epithermal Neutron Activation and Atomic Absorption Spectroscopy in 85 moss samples. The species of moss used in the work was Pleurosium schreberi. Based on the analysis results, the most contaminated areas are identified.

scholarly journals Synthesis and Characterisation of New {Fe2CrO} Heterotrinuclear Iron-chromium Clusters

2021 ◽  
Author(s):  
Viorina Gorinchoy ◽  
Olesea Cuzan ◽  
Silvia Melnic ◽  
Oleg Petuhov ◽  
Sergiu Shova
Keyword(s):  
Thermal Properties ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Elemental Analysis ◽  
Atomic Absorption Spectroscopy ◽  
X Ray ◽  
Heteronuclear Complexes ◽  
The Stability ◽  
Iron Chromium ◽  
Salicylic Acids

Two new μ3-oxo trinuclear heterometallic Fe2IIICrIII complexes with furan-2-carboxylic and salicylic acids with the composition: [Fe2CrO(C4H3OCOO)6(CH3OH)3]NO3·0.5CH3OH and [Fe2CrO(C6H4(OH)COO)7(CH3OH)2]·2DMA were synthesized starting from iron(III) and chromium(III) salts mixture. The complexes structures were confirmed by elemental analysis, IR, Mössbauer spectroscopies, and X-ray analysis. The atomic absorption spectroscopy confirmed that the iron: chromium ratio is 2:1. The thermal properties of both heteronuclear complexes have been investigated in oxidizing and inert atmospheres revealing the stability of the trinuclear core up to 170 and 220°C, respectively.

scholarly journals Elemental Analysis of Paeonia emodi and Punica granatum by Atomic Absorption Spectroscopy

2012 ◽  
Vol 2 (4) ◽  
pp. 47-50 ◽  
Author(s):  
Faizul Haq ◽  
Shamsur Rehman ◽  
Habib Ahmad ◽  
Zafar Iqbal ◽  
Rahat Ullah
Keyword(s):  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Elemental Analysis ◽  
Atomic Absorption Spectroscopy ◽  
Punica Granatum

Hopewell Obsidian Studies: Behavioral Implications of Recent Sourcing and Dating Research

1990 ◽  
Vol 55 (3) ◽  
pp. 461-479 ◽  
Author(s):  
James W. Hatch ◽  
Joseph W. Michels ◽  
Christopher M. Stevenson ◽  
Barry E. Scheetz ◽  
Richard A. Geidel
Keyword(s):  
Neutron Activation Analysis ◽  
Activation Analysis ◽  
Neutron Activation ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Atomic Absorption Spectroscopy ◽  
Compositional Characterization

Specific questions regarding the antiquity of major midwestern Hopewell culture sites and their role in regional exchange systems are addressed in this paper through the dating (obsidian hydration) and compositional characterization (neutron activation analysis [NAA] and atomic absorption spectroscopy [AAS]) of obsidian artifacts. The analysis of 34 specimens from the Seip, Mound City, and Hopewell sites, Ohio, and the Naples site, Illinois, increases fivefold the number of chronometric dates available from these sites and expands the sample of compositionally identified specimens beyond those resulting from Griffin et al."s (1969) pioneering work. The resulting hydration dates support earlier estimates of the age of these contexts based on 14C or artifact seriation alone. The range of dates (78 B.C.-A.D. 347) and the compositional variety within the sample favors an expanded view of the nature of obsidian trade in the Midwest to include additional western sources, a longer episode of importation, and possible changes in the sources used through time.

scholarly journals Determination of trace aluminum concentration and homogeneity in biological reference material TORT-1 by instrumental neutron activation analysis and graphite furnace atomic absorption spectroscopy

1987 ◽  
Vol 65 (5) ◽  
pp. 1047-1050 ◽  
Author(s):  
Byron Kratochvil ◽  
Norine Motkosky ◽  
M. John M. Duke ◽  
Dennis Ng
Keyword(s):  
Neutron Activation Analysis ◽  
Instrumental Neutron Activation Analysis ◽  
Activation Analysis ◽  
Reference Material ◽  
Neutron Activation ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Atomic Absorption Spectroscopy ◽  
Graphite Furnace ◽  
Graphite Furnace Atomic Absorption

The biological reference material TORT-1, lobster hepatopancreas, was analyzed for aluminum by instrumental neutron activation analysis (INAA) and graphite furnace atomic absorption spectroscopy (GFAAS). After correction of the INAA results for interferences from 28Al produced by 31P(n,α)28Al and 28Si(n,p)28Al reactions, and use of HNO3 plus HF for sample dissolution for the GFAAS analyses, the methods gave similar results of 43 ± 3 and 42 ± 2 μg/g respectively for 200 to 300-mg test portions. Analysis of six portions from each of six bottles of TORT-1 showed no statistical difference at the 95% confidence level for the between and within bottle variances. Therefore, the material can be considered homogeneous for aluminum if 200- to 300-mg test portions are taken. The variance was greater and the average lower when 30-mg test portions were analyzed for aluminum by GFAAS. The pattern of the results, together with the need for HF in the dissolution procedure, suggests the presence of aluminum-containing microparticulate mineral matter, perhaps silicate material, in the material.

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