Microwave-assisted, solvent-free, one-pot, three-component synthesis of fused pyran derivatives containing benzothiazole nucleus catalyzed by pyrrolidine-acetic acid and their biological evaluation

2017 ◽  
Vol 148 (6) ◽  
pp. 1057-1067 ◽  
Author(s):  
Haresh B. Patel ◽  
Jayvirsinh D. Gohil ◽  
Manish P. Patel
Keyword(s):  
Acetic Acid ◽  
Biological Evaluation ◽  
Solvent Free ◽  
One Pot ◽  
Microwave Assisted

Microwave-Assisted Efficient, One-Pot, Three-Component Synthesis of 3,5-Disubstituted 1,2,4-Oxadiazoles under Solvent-Free Conditions.

ChemInform ◽  
2006 ◽  
Vol 37 (32) ◽  
Author(s):  
Mehdi Adib ◽  
Amin Haghighat Jahromi ◽  
Narjes Tavoosi ◽  
Mohammad Mahdavi ◽  
Hamid Reza Bijanzadeh
Keyword(s):  
Solvent Free ◽  
One Pot ◽  
Microwave Assisted ◽  
Solvent Free Conditions

[Et3NH][HSO4]-Catalyzed One-Pot Solvent Free Syntheses of Functionalized [1,6]-Naphthyridines and Biological Evaluation

2021 ◽  
pp. 1-17
Author(s):  
Mubarak H. Shaikh ◽  
Dnyaneshwar D. Subhedar ◽  
Vijay M. Khedkar ◽  
Bapurao B. Shingate
Keyword(s):  
Biological Evaluation ◽  
Solvent Free ◽  
One Pot

A Convenient One-Pot and Rapid Microwave-Assisted Synthesis of Biologically Active s-Triazolo[3,4-b][1,3,4]Thiadiazine and s-Triazolo[3,4-b][1,3,4]Thiadiazole Nanoarchitectonics

2020 ◽  
Vol 20 (5) ◽  
pp. 2917-2929
Author(s):  
Ahmed F. M. EL-Mahdy ◽  
Hassan A. H. EL-Sherief ◽  
Zeinab A. Hozien ◽  
Shiao-Wei Kuo
Keyword(s):  
Acetic Acid ◽  
Sulfuric Acid ◽  
Reaction Time ◽  
Catalytic Amount ◽  
Biologically Active ◽  
Microwave Assisted Synthesis ◽  
One Pot ◽  
Microwave Assisted ◽  
Work Up ◽  
Temperature Time

A rapid and efficient one-pot protocol has been developed for the synthesis of s-triazolo[3,4-b][1,3,4]thiadiazine and s-triazolo[3,4-b][1,3,4]thiadiazole nanoarchitectonics through the reaction of s-triazoles with ketones and nitriles in acetic acid containing a catalytic amount of sulfuric acid under microwave irradiation in excellent yields. With this catalytic reaction, the cheap sulfuric acid as well as other acids were examined as catalysts and the highly toxic and irritating haloketones and halonitriles were avoided to form. The effects of microwave power, temperature, time, solvent and catalyst were examined. This method achieved a better performance; e.g., higher yields, shorter reaction time and easier work-up as compared to other conventional methods. Therefore, the proposed method will be readily applicable to the synthesis of biologically important compounds containing s-triazolo[3,4-b][1,3,4]thiadiazine and s-triazolo[3,4-b][1,3,4]thiadiazole framework.

ChemInform Abstract: Solvent-Free, Microwave-Assisted, One-Pot Synthesis of 2-Acetyl-N,3-diaryl-4-nitrobutanamides.

ChemInform ◽  
2011 ◽  
Vol 42 (32) ◽  
pp. no-no
Author(s):  
Issa Yavari ◽  
Saeideh Beheshti ◽  
Zinatossadat Hossaini ◽  
Sanaz Souri
Keyword(s):  
Solvent Free ◽  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis
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