scholarly journals Adsorptive stripping voltammetric method for the determination of caffeine at integrated three-electrode screen-printed sensor with carbon/carbon nanofibers working electrode

Adsorption ◽  
2019 ◽  
Vol 25 (4) ◽  
pp. 913-921 ◽  
Author(s):  
Katarzyna Tyszczuk-Rotko ◽  
Karolina Pietrzak ◽  
Agnieszka Sasal
Fuel ◽  
2013 ◽  
Vol 105 ◽  
pp. 306-313 ◽  
Author(s):  
Ricardo Pini Caramit ◽  
Adriana Garabini de Freitas Andrade ◽  
João Batista Gomes de Souza ◽  
Tatiane Alfonso de Araujo ◽  
Luiz Henrique Viana ◽  
...  

2019 ◽  
Vol 11 (35) ◽  
pp. 4494-4500 ◽  
Author(s):  
Abd-Elgawad Radi ◽  
Alsayed Eissa ◽  
Tarek Wahdan

A voltammetric method at a single walled carbon nanotube screen-printed electrode was applied for the determination of zearalenone in food samples.


2020 ◽  
Vol 32 (7) ◽  
pp. 1618-1628 ◽  
Author(s):  
Agnieszka Sasal ◽  
Katarzyna Tyszczuk‐Rotko ◽  
Michał Chojecki ◽  
Tatiana Korona ◽  
Agnieszka Nosal‐Wiercińska

2005 ◽  
Vol 70 (5) ◽  
pp. 735-743 ◽  
Author(s):  
Valeria Guzsvány ◽  
Ferenc Gaál ◽  
Luka Bjelica ◽  
Silvija Ökrész

A simple voltammetric method using a glassy carbon working electrode was developed for the determination of two members from the neonicotinoid group of insecticides: imidacloprid and thiamethoxam. The experiments showed that the voltammetric response depends on the mode of electrode surface pretreatment and the polarization mode. The response appeared to be linear in the range from 0.028 to 0.50 mg/cm3 for both analyses. The limit of detection was 0.0077 mg/cm3 for imidacloprid and 0.0085 mg/cm3 for thiamethoxam, the limit of quantitation was 0.026 mg/cm3 and 0.028 mg/cm3, respectively. The developed method was applied for the determination of these insecticides in potato samples sprayed with Confidor 200-SL or Actara 25-WG as well as commercial formulations of imidacloprid and thiamethoxam. A recovery trial was performed to assess the accuracy of the results, the recovery values being between 95?102 % for both of neonicotinoids.


1991 ◽  
Vol 56 (3) ◽  
pp. 595-601 ◽  
Author(s):  
Jiří Barek ◽  
Gulamustafa Malik ◽  
Jiří Zima

Optimum conditions were found for the determination of 4-nitrobiphenyl by fast scan differential pulse voltammetry at a hanging mercury drop electrode in the concentration range 1 . 10-5 to 2 . 10-7 mol l-1. A further increase in sensitivity was attained by adsorptive accumulation of this substance on the surface of the working electrode, permitting determination in the concentration range (2 – 10) . 10-8 mol l-1 with one minute accumulation of the substance in unstirred solution or (2 – 10) . 10-9 mol l-1 with three-minute accumulation in stirred solution. Linear scan voltammetry can be used to determine 4-nitrobiphenyl in the concentration range (2 – 10) . 10-9 mol l-1 with five-minute accumulation in stirred solution, with the advantage of a smoother baseline and smaller interference from substances that yield only tensametric peaks.


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