Local Structure, Thermal, Optical and Electrical Properties of LiFePO4 Polycrystalline Synthesized by Co-Precipitation Method

Author(s):  
Mouna Sellami ◽  
Maud Barre ◽  
Mohamed Dammak ◽  
Mohamed Toumi
2011 ◽  
Author(s):  
Japinder Kaur ◽  
Tsering Namgyal ◽  
Sandeep Bansal ◽  
Sonal Singhal ◽  
S. K. Tripathi ◽  
...  

CrystEngComm ◽  
2014 ◽  
Vol 16 (17) ◽  
pp. 3584-3591 ◽  
Author(s):  
M. Gopalakrishnan ◽  
V. Purushothaman ◽  
V. Ramakrishnan ◽  
G. M. Bhalerao ◽  
K. Jeganathan

Nitridation at high temperature enhances the crystalline and optical quality of GaN nanoparticles synthesized by a novel chemical co-precipitation method.


2017 ◽  
Vol 28 (12) ◽  
pp. 8655-8661 ◽  
Author(s):  
Xianxian Xie ◽  
Mingxing Chen ◽  
Ting Liu ◽  
Hui Jiang ◽  
Huimin Zhang ◽  
...  

2020 ◽  
Vol 761 ◽  
pp. 137989
Author(s):  
Tariq Munir ◽  
Naeem ur Rehman ◽  
Arslan Mahmood ◽  
Khalid Mahmood ◽  
Adnan Ali ◽  
...  

2007 ◽  
Vol 311 (2) ◽  
pp. 494-499 ◽  
Author(s):  
I.H. Gul ◽  
A.Z. Abbasi ◽  
F. Amin ◽  
M. Anis-ur-Rehman ◽  
A. Maqsood

2022 ◽  
Vol 9 (1) ◽  
pp. 105-118
Author(s):  
Endi Suhendi ◽  
◽  
Andini Eka Putri ◽  
Muhamad Taufik Ulhakim ◽  
Andhy Setiawan ◽  
...  

<abstract> <p>In this study, we used a natural resource, yarosite minerals, as a Fe<sub>2</sub>O<sub>3</sub> precursor. Yarosite minerals were used for the synthesis of LaFeO<sub>3</sub>/Fe<sub>2</sub>O<sub>3</sub> doped with ZnO via a co-precipitation method using ammonium hydroxide, which produced a light brown powder. Then, an ethanol gas sensor was prepared using a screen-printing technique and characterized using gas chamber tools at 100,200, and 300 ppm of ethanol gas to investigate the sensor's performance. Several factors that substantiate electrical properties such as crystal and morphological structures were also studied using X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM), respectively. The crystallite size decreased from about 61.4 nm to 28.8 nm after 0.5 mol% ZnO was added. The SEM characterization images informed that the modified LaFeO<sub>3</sub> was relatively the same but not uniform. Lastly, the sensor's electrical properties exhibited a high response of about 257% to 309% at an operating temperature that decreased from 205 ℃ to 180 ℃. This finding showed that these natural resources have the potential to be applied in the development of ethanol gas sensors in the future. Hence, yarosite minerals can be considered a good natural resource that can be further explored to produce an ethanol gas sensor with more sensitive response. In addition, this method reduces the cost of material purchase.</p> </abstract>


2021 ◽  
Vol 1028 ◽  
pp. 84-89
Author(s):  
Mohammad Syaiful Anwar ◽  
Kharisma Noor Afifah Supoyo ◽  
Retno Asih ◽  
Malik Anjelh Baqiya ◽  
Prae Chirawatkul ◽  
...  

Cu-doped ZnO (CZO) with Cu %mole of 0, 13, 14, and 15% have been synthesized by the co-precipitation method with controlled pH at 9. The diffraction pattern of CZO shows that a single phase of ZnO with wurtzite structure (w-ZnO) was achieved in the parent compound. In contrast, small fractions of the secondary phase of CuO monoclinic (m-CuO) were identified in the doped compounds. Rietveld-refinement on the X-Ray Diffraction (XRD) patterns reveals that the crystallite size of CZO is estimated in the range of 84 - 148 nm with instrumental correction factor and that CZO14 exhibits the most considerable fraction of m-CuO among the samples. Interestingly, lattice constants decrease by Cu doping. The effects of Cu doping on the valence state and the local structure were investigated by X-Ray Absorption Spectroscopy (XAS). Based on our analysis on both Cu K-edge and Zn K-edge XANES spectra, oxidation states of Cu and Zn ions are about +2 with no evidence of other valence states. Cu atom is likely to incorporate into wurtzite crystal lattice by occupying Zn sites in a small portion, and the doped compounds create a few oxygen vacancies.


Sign in / Sign up

Export Citation Format

Share Document