Spectrophotometric determination of lead with 1-(2-pyridylazo)-2-naphthol and non-ionic surfactants Application to acetic acid extracts of ceramic enamels

Talanta ◽  
1985 ◽  
Vol 32 (11) ◽  
pp. 1058-1060 ◽  
Author(s):  
J Escriche
1970 ◽  
Vol 53 (3) ◽  
pp. 582-584
Author(s):  
F Raymond Fazzari

Abstract A method has been developed for the determination of benzthiazide, hydrochlorothiazide, and hydroflumethiazide in pharmaceuticals. The procedure is rapid and specific and employs established separation techniques. The active ingredient is eluted from a basic Celite column with an acetic acid-ether solvent and extracted from the organic phase into NaOH for the spectrophotometric determination.


Talanta ◽  
1978 ◽  
Vol 25 (11-12) ◽  
pp. 691-692 ◽  
Author(s):  
P. Nenova ◽  
D. Kantcheva ◽  
B. Karadakov

1969 ◽  
Vol 52 (4) ◽  
pp. 831-832
Author(s):  
Sandra J Bell

Abstract Batches of 3,3’-dichloroindanthrene meeting the specifications set forth in the Color Additive Regulations are certifiable as D&C Blue No. 9. One of the specifications requires that D&C Blue No. 9 contain no more than 0.2% 2-aminoanthraquinone. In the method described, 2-aminoanthraquinone is extracted from D&C Blue No. 9 with dimethylsulfoxide, together with several other impurities. This solution is spotted onto a thin layer plate and developed with diethyl ether. After removal from t he plate, the 2-aminoanthraquinone is extracted into acetic acid and the amount is determined spectrophotometrically. Recoveries of 0.1, 0.2, and 0.5% of added intermediate ranged from 86 to 96%.


1983 ◽  
Vol 28 (1) ◽  
pp. 77-81 ◽  
Author(s):  
Wadala A. Bashir ◽  
Ghazar W. Hagop ◽  
S. Flamerz

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