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2022 ◽  
Vol 8 (4) ◽  
pp. 270-279
Anup K Chakraborty ◽  
Harshita Tripathi ◽  
Sarita Karole ◽  
Kavita R Loksh

is a significant therapeutic plant has a place with family apocynaceae contains in excess of 70 distinct sorts of chemotherapeutic agents and alkaloids which help in treating different illnesses. For the most part, it is known as Vincarosea, Ammocallisrosea and Lochnerarosea. There are numerous or more than 400 alkaloids present in plant, which are used as flavor, agrochemicals, pharmaceuticals, fragrance, ingredients, food addictives, and pesticides. To develop a validated high performance thin layer chromatographic method for the analysis of leaves and flower extracts of Sample solutions were applied onto the plates with automatic TLC sampler Linomat V (Camag, Muttenz, Switzerland) and were controlled by WinCATS software. Plates were developed in 10 x 10cm twin trough glass chamber (Camag, Muttenz, Switzerland). A CAMAG TLC scanner was used for scanning the TLC plates. Pre-coated silica gel aluminium plates 60F254. For vincristine, simultaneous estimation of vincristine was performed by HPTLC on a silica gel plate using toluene-methanol-diethylamine (8.75: 0.75: 0.5, v/v/v) as the mobile phase. The method was validated as per the ICH guidelines. The Rf value was found to be 0.76 for flower and 0.80 for leaves at 250 nm which shows the presence of vincristin in . In this research paper, a validated HPTLC Method has been developed for the analysis of leaves and flower extracts

2022 ◽  
pp. 1-10
Dong Hyun Kim ◽  
Eun-Mi Kim ◽  
Gi-Seok Heo ◽  
Dong Wook Lee ◽  
Jin Young Oh ◽  

2022 ◽  
Vol 7 (1) ◽  
pp. 101-106
Ernest Beinrohr ◽  
Stanislava Hlubikova ◽  
Jarka Lastincova

Flow through coulometry is used for analysis of wine samples for the determination of some heavy metals, sulphites, acidity and ethanol content. Low concentrations of heavy metals and sulphite contents are determined by making use of stripping chronopotentiometry. For the measurement of acid and ethanol content thin-layer coulometric titration is used.

Wenyuan Zhang ◽  
Haojun Xu ◽  
Binbin Pei ◽  
Xiaolong Wei ◽  
Pei Feng ◽  

Abstract This work proposes a new plasma super-phase gradient metasurfaces (PS-PGMs) structure, owing to the limitations of the thin-layer plasma for electromagnetic wave attenuation. Based on the cross-shaped surface unit configuration, we have designed the X-band absorbing structure through the dispersion control method. By setting up the Drude dispersion model in the computer simulation technology, the designed phase gradient metasurfaces structure is superposed over the plasma, and the PS-PGMs structure is constructed. The electromagnetic scattering characteristics of the new structure have been simulated, and the reflectance measurement has been carried out to verify the absorbing effect. The results demonstrate that the attenuation effect of the new structure is superior to that of the pure plasma structure, which invokes an improved attenuation effect from the thin layer plasma, thus enhancing the feasibility of applying the plasma stealth technology to the local stealth of the strong scattering part of a combat aircraft.

2022 ◽  
Vol 350 (1) ◽  
pp. 27-45
Christian Licht ◽  
Somsak Orankitjaroen ◽  
Thibaut Weller

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