An accelerator mass spectrometry system with the 12UD Pelletron at the University of Tsukuba

Author(s):  
Y. Nagashima ◽  
H. Shioya ◽  
Y. Tajima ◽  
T. Takahashi ◽  
T. Kaikura ◽  
...  
Radiocarbon ◽  
1983 ◽  
Vol 25 (2) ◽  
pp. 755-760 ◽  
Author(s):  
G W Farwell ◽  
P M Grootes ◽  
D D Leach ◽  
F H Schmidt

During the past year we have continued to work toward greater stability and flexibility in nearly all elements of our accelerator mass spectrometry (AMS) system, which is based upon an FN tandem Van de Graaff accelerator, and have carried out measurements of 14C/12C and 10Be/9Be isotopic abundance ratios in natural samples. The principal recent developments and improvements in the accelerator system and in our sample preparation techniques for carbon and beryllium are discussed, and the results of a study of 10Be cross-contamination of beryllium samples in the sputter ion source are presented.


Radiocarbon ◽  
2021 ◽  
pp. 1-7
Author(s):  
Corina Solís ◽  
Efraín Chávez ◽  
Arcadio Huerta ◽  
María Esther Ortiz ◽  
Alberto Alcántara ◽  
...  

ABSTRACT Augusto Moreno is credited with establishing the first radiocarbon (14C) laboratory in Mexico in the 1950s, however, 14C measurement with the accelerator mass spectrometry (AMS) technique was not achieved in our country until 2003. Douglas Donahue from the University of Arizona, a pioneer in using AMS for 14C dating, participated in that experiment; then, the idea of establishing a 14C AMS laboratory evolved into a feasible project. This was finally reached in 2013, thanks to the technological developments in AMS and sample preparation with automated equipment, and the backing and support of the National Autonomous University of Mexico and the National Council for Science and Technology. The Mexican AMS Laboratory, LEMA, with a compact 1 MV system from High Voltage Engineering Europa, and its sample preparation laboratories with IonPlus automated graphitization equipment, is now a reality.


2011 ◽  
Author(s):  
W. E. Kieser ◽  
X.-L. Zhao ◽  
I. D. Clark ◽  
T. Kotzer ◽  
A. E. Litherland ◽  
...  

Author(s):  
Seiji Hosoya ◽  
Kimikazu Sasa ◽  
Tsutomu Takahashi ◽  
Tetsuya Matsunaka ◽  
Masumi Matsumura ◽  
...  

Radiocarbon ◽  
2004 ◽  
Vol 46 (1) ◽  
pp. 83-88 ◽  
Author(s):  
L Wacker ◽  
M Grajcar ◽  
S Ivy-Ochs ◽  
PW Kubik ◽  
M Suter

The injection of 10BeF- instead of 10BeO- into a compact accelerator mass spectrometry system with a terminal voltage of 0.58 MV was investigated, because BF- molecules are unstable and isobaric interference of 10B with 10Be can thus be significantly reduced. We describe the method we developed to prepare BeF2 samples. 10Be was measured in a segmented gas ionization detector. Separation of 10Be from 10B could be achieved both for ions in the 1+ charge state with an energy of 0.8 MeV and in the 2+ charge state with an energy of 1.4 MeV. The 2+ ions are better separated, whereas the 1+ charge state has a higher transmission. 10Be/9Be ratios (~10-12) in a suite of rock samples were successfully determined for exposure dating in either charge state and compared with measurements made on the 6MV tandem.


Radiocarbon ◽  
2010 ◽  
Vol 52 (2) ◽  
pp. 301-309 ◽  
Author(s):  
Robert K Beverly ◽  
Will Beaumont ◽  
Denis Tauz ◽  
Kaelyn M Ormsby ◽  
Karl F von Reden ◽  
...  

We present a status report of the accelerator mass spectrometry (AMS) facility at the University of California, Irvine, USA. Recent spectrometer upgrades and repairs are discussed. Modifications to preparation laboratory procedures designed to improve sample throughput efficiency while maintaining precision of 2–3‰ for 1-mg samples (Santos et al. 2007c) are presented.


Radiocarbon ◽  
1987 ◽  
Vol 29 (3) ◽  
pp. 323-333 ◽  
Author(s):  
J S Vogel ◽  
D E Nelson ◽  
J R Southon

The levels and sources of the measurement background in an AMS 14C dating system have been studied in detail. The relative contributions to the total background from combustion, graphitization, storage, handling, and from the accelerator were determined by measuring the C concentrations in samples of anthracite coal ranging in size from 15μg to 20mg. The results show that, for the present system, the uncertainty in the background is greater than that due to measurement precision alone for very old or for very small samples. While samples containing 100μg of carbon can yield useful 14C dates throughout the Holocene, 200 to 500μg are required for dating late Pleistocene materials. With the identification of the procedures that introduce contamination, the level and uncertainty of the total system background should both be reducible to the point that 100μg of carbon would be sufficient for dating most materials.


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