Sensitive capillary gas chromatographic-mass spectrometric-selected-ion monitoring method for the determination of diclofenac concentrations in human plasma

Author(s):  
Michael R. Borenstein ◽  
Yuzhu Xue ◽  
Stephen Cooper ◽  
Tsang-Bin Tzeng
1991 ◽  
Vol 74 (5) ◽  
pp. 815-818
Author(s):  
Shigeru Tan ◽  
Takashi Tatsuno ◽  
Taro Okada

Abstract A selected ion monitoring method is described for the analysis of styrene (St)-based polymers for a-methylstyrene (α- MSt) and for determining the level of α-MSt migration from St-based sheets Into 4 food simulants. The polymers are dissolved in dlchloromethane; α-MSt Is determined by direct Injection of the polymer solutions. α-MSt migration from St-based sheet to water, 4% acetic acid, 20% ethanol, and n-heptane was measured by gas chromatography/mass spectrometry, using multiple ion monitoring of Ions at mix 118,78, and 91. α-MSt can be quantltated at levels as low as 10 μ/g in the polymer and 0.01 μ/g In the food simulants. Recoveries were 83-113% from St-based sheets and 90-99% from food simulants, respectively.


2002 ◽  
Vol 776 (1) ◽  
pp. 107-113 ◽  
Author(s):  
Tetsuya Arinobu ◽  
Hideki Hattori ◽  
Masae Iwai ◽  
Akira Ishii ◽  
Takeshi Kumazawa ◽  
...  

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