Debranched cassava starch crystallinity determination by Raman spectroscopy: Correlation of features in Raman spectra with X-ray diffraction and 13C CP/MAS NMR spectroscopy

2012 ◽  
Vol 87 (1) ◽  
pp. 598-606 ◽  
Author(s):  
Christopher Mutungi ◽  
Lars Passauer ◽  
Calvin Onyango ◽  
Doris Jaros ◽  
Harald Rohm
2004 ◽  
Vol 357 (9) ◽  
pp. 2510-2518 ◽  
Author(s):  
Anna-Carin Larsson ◽  
Alexander V Ivanov ◽  
Oleg N Antzutkin ◽  
Andrey V Gerasimenko ◽  
Willis Forsling

1999 ◽  
Vol 322 (3-4) ◽  
pp. 256-263 ◽  
Author(s):  
Hiroyuki Kono ◽  
Yukari Numata ◽  
Nobuhiro Nagai ◽  
Tomoki Erata ◽  
Mitsuo Takai

2014 ◽  
Vol 92 (6) ◽  
pp. 542-548 ◽  
Author(s):  
Lucian-Cristian Pop ◽  
Nobuaki Kurokawa ◽  
Hiroaki Ebata ◽  
Katsuya Tomizawa ◽  
Tomoyuki Tajima ◽  
...  

The first stable stannanetriol and germanetriol bearing sterically congested aryl groups were synthesized by hydrolysis of the corresponding trichloro-stannane and -germane. The stannanetriol is monomeric in solution as well as in the crystalline state, as evidenced by X-ray diffraction analysis and CP-MAS NMR spectroscopy. The stannanetriol reacted with silicone grease to afford a cagelike compound having three Sn–O–Si–O–Sn linkages in the molecule. All the group 14 triols can be converted to the corresponding trihalo compounds in good yields.


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