X-ray crystallography and solution NMR spectroscopy characterization of heptakis(2,3-di-O-acetyl-6-bromo-6-deoxy)cyclomaltoheptaose

2004 ◽  
Vol 339 (6) ◽  
pp. 1189-1194 ◽  
Author(s):  
Petros Giastas ◽  
Kyriaki Eliadou ◽  
Zoi F. Plyta ◽  
Konstantina Yannakopoulou ◽  
Irene M. Mavridis
Keyword(s):  
Nmr Spectroscopy ◽  
Solution Nmr ◽  
X Ray ◽  
X Ray Crystallography ◽  
Solution Nmr Spectroscopy

Computational challenges for macromolecular structure determination by X-ray crystallography and solution NMRspectroscopy

1993 ◽  
Vol 26 (1) ◽  
pp. 49-125 ◽  
Author(s):  
Axel T. Brünger ◽  
Michael Nilges
Keyword(s):  
Nmr Spectroscopy ◽  
Structure Determination ◽  
Solution Nmr ◽  
Macromolecular Structure ◽  
X Ray ◽  
X Ray Crystallography ◽  
The Past ◽  
Solution Nmr Spectroscopy

Macromolecular structure determination by X-ray crystallography and solution NMR spectroscopy has experienced unprecedented growth during the past decade.

scholarly journals Characterization of the insertase BamA in three different membrane mimetics by solution NMR spectroscopy

2015 ◽  
Vol 61 (3-4) ◽  
pp. 333-345 ◽  
Author(s):  
Leonor Morgado ◽  
Kornelius Zeth ◽  
Björn M. Burmann ◽  
Timm Maier ◽  
Sebastian Hiller
Keyword(s):  
Nmr Spectroscopy ◽  
Solution Nmr ◽  
Solution Nmr Spectroscopy

Characterization of Mercury(II) Complexes of Bis[(2-pyridyl)methyl]amine by X-ray Crystallography and NMR Spectroscopy

1998 ◽  
Vol 37 (12) ◽  
pp. 2952-2959 ◽  
Author(s):  
Deborah C. Bebout ◽  
Anne E. DeLanoy ◽  
David E. Ehmann ◽  
Margaret E. Kastner ◽  
Damon A. Parrish ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
X Ray ◽  
X Ray Crystallography ◽  
Methyl Amine

Preparation, Crystal Structure and Spectroscopic Characterization of [Ga(OH)(SO4)(terpy)(H2O)] · H2O (terpy=2,2’:6’,2-Terpyridine): The First Characterized Gallium(III) Sulfato Complex

2004 ◽  
Vol 59 (3) ◽  
pp. 291-297 ◽  
Author(s):  
Andreas Sofetis ◽  
Giannis S. Papaefstathiou ◽  
Aris Terzis ◽  
Catherine P. Raptopoulou ◽  
Theodoros F. Zafiropoulos
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Nmr Spectroscopy ◽  
Good Yield ◽  
Spectroscopic Data ◽  
Spectroscopic Characterization ◽  
X Ray ◽  
X Ray Crystallography ◽  
H Nmr

The reaction of Ga2(SO4)3·18H2O and excess 2,2′:6′,2″-terpyridine (terpy) in MeOH / H2O leads to [Ga(OH)(SO4)(terpy)(H2O)]·H2O (1·H2O] in good yield. The structure of the complex has been determined by single-crystal X-ray crystallography. The GaIII atom in 1·H2O is 6-coordinate and ligation is provided by one terdentate terpy molecule, one monodentate sulfate, one terminal hydroxide and one terminal H2O molecule; the coodination polyhedron about the metal is described as a distorted octahedron. There is an extensive hydrogen-bonding network in the crystal structure which generates corrugated layers parallel to bc. The new complex was characterized by IR and 1H NMR spectroscopy. The spectroscopic data are discussed in terms of the nature of bonding

scholarly journals Binding Mode Characterization of Osteopontin on Hydroxyapatite by Solution NMR Spectroscopy

ChemBioChem ◽  
2021 ◽  
Author(s):  
Julian Holzinger ◽  
Harald Kotisch ◽  
Klaus W. Richter ◽  
Robert Konrat
Keyword(s):  
Nmr Spectroscopy ◽  
Binding Mode ◽  
Solution Nmr ◽  
Solution Nmr Spectroscopy
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