Homonuclear dipolar decoupling with very large scaling factors for high-resolution ultrafast magic angle spinning 1H solid-state NMR spectroscopy

2010 ◽  
Vol 498 (1-3) ◽  
pp. 214-220 ◽  
Author(s):  
Elodie Salager ◽  
Jean-Nicolas Dumez ◽  
Robin S. Stein ◽  
Stefan Steuernagel ◽  
Anne Lesage ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Scaling Factors ◽  
Solid State Nmr Spectroscopy ◽  
Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

A unified heteronuclear decoupling strategy for magic-angle-spinning solid-state NMR spectroscopy

2015 ◽  
Vol 142 (18) ◽  
pp. 184201 ◽  
Author(s):  
Asif Equbal ◽  
Morten Bjerring ◽  
P. K. Madhu ◽  
Niels Chr. Nielsen
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Solid State Nmr Spectroscopy ◽  
Angle Spinning
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