Effects of annealing temperature variation on the evolution of structural and magnetic properties of NiFe2O4 nanoparticles synthesized by starch-assisted sol–gel auto-combustion method

2015 ◽  
Vol 394 ◽  
pp. 439-447 ◽  
Author(s):  
Raghvendra Singh Yadav ◽  
Jaromir Havlica ◽  
Jiri Masilko ◽  
Lukas Kalina ◽  
Jaromir Wasserbauer ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Temperature Variation ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Combustion Method ◽  
Auto Combustion ◽  
Nife2o4 Nanoparticles ◽  
Structural And Magnetic Properties

Structural and magnetic properties of Cr doped strontium spinel ferrite SrFe2O4 by sol-gel auto-combustion method

2018 ◽  
Vol 550 ◽  
pp. 90-95 ◽  
Author(s):  
Nazia Yasmin ◽  
Iqra Inam ◽  
Iftikhar Ahmed Malik ◽  
Maria Zahid ◽  
Muhammad Naeem Ashiq ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Spinel Ferrite ◽  
Sol Gel ◽  
Combustion Method ◽  
Auto Combustion ◽  
Structural And Magnetic Properties

Effect of annealing temperature on structural and magnetic properties of strontium hexaferrite nanoparticles synthesized by sol–gel auto-combustion method

2015 ◽  
Vol 29 (27) ◽  
pp. 1550190 ◽  
Author(s):  
Ebrahim Roohani ◽  
Hadi Arabi ◽  
Reza Sarhaddi ◽  
Saeedeh Sudkhah ◽  
Ameneh Shabani
Keyword(s):  
Crystal Structure ◽  
Thermal Decomposition ◽  
Magnetic Properties ◽  
Thermogravimetric Analysis ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Combustion Method ◽  
Strontium Hexaferrite ◽  
Auto Combustion ◽  
Ft Ir

In this paper, strontium hexaferrite nanoparticles were synthesized by the sol–gel auto-combustion method. Effect of annealing temperature on crystal structure, morphology and magnetic properties of nanoparticles was investigated by X-ray diffraction (XRD), Fourier transform infrared (FT-IR), transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM). Also, the thermal decomposition of as-synthesized powdered samples has been studied by thermogravimetric analysis (TGA). The XRD patterns confirmed the formation of single phase M-type hexagonal crystal structure for powders annealed above 950[Formula: see text]C, whereas the presence of hematite ([Formula: see text]-Fe2O3) as secondary phase was also observed for sample annealed at 900[Formula: see text]C. Furthermore, the crystallinity along with the crystallite size were augmented with annealing temperature. Comparison of the FT-IR spectra of the samples before and after annealing treatment showed the existence of metal–oxygen stretching modes after annealing. The thermogravimetric analysis confirmed the thermal decomposition of as-burnt powders happened in three-stage degradation process. The TEM images showed the nanoparticles like hexagonal-shaped platelets as the size of nanoparticles increases by increasing the annealing temperature. With increasing annealing temperature, the magnetic saturation and the coercivity were increased to the maximum value of 74.26 emu/g and 5.67 kOe for sample annealed at 1000[Formula: see text]C and then decreased.

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